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Journal articles on the topic 'X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD)'

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Published: 2 June 2025

Last updated: 31 July 2025

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1

Kerner, Jonathan A., Edward D. Franco, and John Marshall. "Combined XRD and XRF Analysis for Portable and Remote Applications." Advances in X-ray Analysis 38 (1994): 319–24. http://dx.doi.org/10.1154/s037603080001795x.

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Abstract A prototype instrument, which provides x-ray powder diffraction and x-ray fluorescence analysis in a compact unit, has been developed to support the needs of NASA for planetary exploration. The instrument uses a 9-watt Fe-anodc x-ray tube and CCD in a fixed geometry for recording powder patterns with a 2θ range of 35°. The fluorescence spectrum for elements below Fe is collected simultaneously with the diffraction data. A shuttered Cd-109 isotopic source with emissions at 22 and 80 keV is used to excite higher energy fluorescence. The low-energy limit for discriminating single photon

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Gurker, N. "Imaging Techniques for X-Ray Fluorescence and X-Ray Diffraction." Advances in X-ray Analysis 30 (1986): 53–65. http://dx.doi.org/10.1154/s0376030800021145.

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Electron induced X-ray mapping together with modern SEM/EDX analysis systems has reached a high level of perfection due to established methods of beam deflection and focusing and today's standard in energy dispersive X-ray detection and data processing. X-ray analysis of specimens based on X-ray excitation (XRF/XRD) is routinely performed on comparatively large specimen areas without conserved spatial information. XRF-/XRD-imaging capabilities are not yet commonly available on standard spectrometers, since both suitable X-ray optical elements are missing and there is a large intensity loss due

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Chung, Frank H. "Quantitative X-ray diffraction and X-ray fluorescence analyses of mixtures – unified and simplified." Journal of Applied Crystallography 51, no. 3 (2018): 789–95. http://dx.doi.org/10.1107/s1600576718005228.

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Owing to the complex matrix effects, the current approach to quantitative X-ray diffraction (XRD) and X-ray fluorescence (XRF) analyses of mixtures requires calibration lines from standards, and is hence tedious and time consuming. New insights reveal that both the matrix effects and the calibration lines can be eliminated mathematically. Any complex mixture can be transformed into a set of simple binary mixtures. One straightforward formula decodes both XRD and XRF. A single XRD or XRF scan quantifies the chemical compounds or chemical elements in any mixture. The unified and simplified proce

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Bortolotti, M., L. Lutterotti, and G. Pepponi. "Combining XRD and XRF analysis in one Rietveld-like fitting." Powder Diffraction 32, S1 (2017): S225—S230. http://dx.doi.org/10.1017/s0885715617000276.

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X-ray diffraction (XRD) and X-ray fluorescence (XRF) are widely used analytical techniques for materials characterization; the information they provide can be considered complementary, as the former is mostly used to obtain crystallographic information and analyze phase content, whereas the latter is sensitive to elemental composition. Many researchers and technologists working in a variety of application fields already use them together in some sort of a “combined” approach, by separately performing XRD and XRF data collection and analysis on the same sample and then comparing the analytical

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Chung, Frank H. "Unified Theory for Decoding the Signals from X-Ray Florescence and X-Ray Diffraction of Mixtures." Applied Spectroscopy 71, no. 5 (2016): 1060–68. http://dx.doi.org/10.1177/0003702816664105.

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For research and development or for solving technical problems, we often need to know the chemical composition of an unknown mixture, which is coded and stored in the signals of its X-ray fluorescence (XRF) and X-ray diffraction (XRD). X-ray fluorescence gives chemical elements, whereas XRD gives chemical compounds. The major problem in XRF and XRD analyses is the complex matrix effect. The conventional technique to deal with the matrix effect is to construct empirical calibration lines with standards for each element or compound sought, which is tedious and time-consuming. A unified theory of

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Abubaker, Shawbo A., Faten A. Chaqmaqchee, and Akram H. Taha. "Identification and Characterization of Different Types of Plastics Wastes Using X-Ray Diffraction and X-Ray Fluorescence Techniques." ARO-THE SCIENTIFIC JOURNAL OF KOYA UNIVERSITY 9, no. 2 (2021): 22–25. http://dx.doi.org/10.14500/aro.10840.

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In this study, different types of polymers in postconsumer plastics with pure plastics have been studied. Highdensity polyethylene (HDPE1 and HDPE2), polyvinyl chloride (PVC3 and PVC4), polyethylene terephthalate (PET5 and PET6), and polypropylenes (PP7 and PP8) were compared using X-ray diffraction (XRD) and X-ray fluorescence (XRF) techniques. XRF has shown the spectral in K-lines of polymer materials present in plastics waste. The peak intensity and degree of crystallinity of commercial polymers are varied using XRD analysis. The intensity not attributable to the crystalline peaks may be re

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Söğüt, Ö., Ç. Dönük, G. Apaydın, and Ö. F. Bakkaloğlu. "Examination of CoNiCu thin films by using XRF and XRD." Canadian Journal of Physics 92, no. 5 (2014): 435–39. http://dx.doi.org/10.1139/cjp-2012-0538.

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A series of thin films of CoNiCu and NiCu produced using the electrodeposition method have been examined using X-ray fluorescence (XRF), X-ray diffraction (XRD), and scanning electron microscopy (SEM). Energy dispersive XRF spectroscopy was used to determine the concentrations of the atomic percentage in these films. CoNiCu and NiCu thin film samples were excited by gamma rays with 59.5 keV energy photons from 100 mCi 241Am radioisotope source. K X-rays emitted by samples were counted by an Ultra-LEGe detector having a resolution of 150 eV at 5.9 keV. Structural analyses of these films have be

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He, Z., Y. J. Xu, N. Huang, et al. "Optimization of parameters for portable X-ray diffraction/X-ray fluorescence combined analysis device (P-XRDF-CAD)." Journal of Instrumentation 18, no. 09 (2023): P09027. http://dx.doi.org/10.1088/1748-0221/18/09/p09027.

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Abstract This paper aims to optimize the parameters of a portable device that combines X-ray diffraction (XRD) and X-ray fluorescence (XRF) analysis techniques. By using the same X-ray source and detector, the device enables the simultaneous acquisition of two-dimensional XRD and XRF information from a sample with the advantage of high analysis efficiency and consistency in the measurement points. The equipment and slit materials are discussed, including the selection of the X-ray source (Moxtek MAGNUM) and the detector (Andor CCD camera). We also explore two different slit designs (the bottom

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Sandeepan, Saha*1 &. Prof. Dr. Sumit Kr. Biswas2. "A STUDY BETWEEN STRUCTURAL CORRELATION &MECHANICAL PROPERTIES OF SUB-GRADE SOIL WHEN BLENDED WITH LIME AND RICE HUSK ASH." INTERNATIONAL JOURNAL OF ENGINEERING SCIENCES & RESEARCH TECHNOLOGY 8, no. 8 (2019): 23–31. https://doi.org/10.5281/zenodo.3360454.

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Present study considers structural characterization of sub-grade soil to increase the strength of soil for road. The present investigation has been carried out with agricultural waste materials like Rice Husk Ash individually mixed with soil and also in combination with different percentage of Hydrated Lime. Structural and mechanical characterization of the investigated samples was performed by X-Ray Diffraction (XRD), X-Ray Fluorescence (XRF), Standard Proctor Test, Unconfined Compression Test, California Bearing Ratio (CBR)Test. It was observed that increase of strength may be due to the red

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Sabri, Mohammed M. "Chemical and Structural Analysis of Rocks Using X-ray Fluorescence and X-ray Diffraction Techniques." ARO-THE SCIENTIFIC JOURNAL OF KOYA UNIVERSITY 8, no. 1 (2020): 79–87. http://dx.doi.org/10.14500/aro.10643.

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Rock examinations for mining and commercial use are a vital process to save money and time. A variety of methods and approaches have been used to analyze rocks and among them, X-ray fluorescence (XRF), and X-ray diffraction (XRD) techniques proved to be an accurate method. This research was conducted to evaluate the utility and reliability of XRF and XRD to analyze the major and trace elements of rocks as well as their crystalline structures. Results showed that XRF and XRD techniques are fast and reliable, nondestructive and non-invasive analytical tools for mineral analysis, particularly for

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Eveno, Myriam, Brice Moignard, and Jacques Castaing. "Portable Apparatus for In Situ X-Ray Diffraction and Fluorescence Analyses of Artworks." Microscopy and Microanalysis 17, no. 5 (2011): 667–73. http://dx.doi.org/10.1017/s1431927611000201.

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AbstractA portable X-ray fluorescence/X-ray diffraction (XRF/XRD) system for artwork studies has been designed constructed and tested. It is based on Debye Scherrer XRD in reflection that takes advantage of many recent improvements in the handling of X-rays (polycapillary optics; advanced two-dimensional detection). The apparatus is based on a copper anode air cooled X-ray source, and the XRD analysis is performed on a 5–20 μm thick layer from the object surface. Energy dispersive XRF elemental analysis can be performed at the same point as XRD, giving elemental compositions that support the i

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Ariyanto, Sandy Vikki, Idon Joni, and Fredy Yunanto. "XRF AND XRD TESTING FOR SAND MINERAL CONTENT IDENTIFICATION AT TALANG SIRING BEACH." EduFisika: Jurnal Pendidikan Fisika 8, no. 2 (2023): 226–32. http://dx.doi.org/10.59052/edufisika.v8i2.27428.

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In the Talang siring tour of the Pamekasan district, numerous illegal mining operations along the coast for sale and personal use produce building materials with low economic value. However, if the sand is processed further, it will produce materials with high technology utilization and economic value. This research is a preliminary investigation into converting sand into high-value minerals to be utilized economically. Using X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD) experiments, this study aims to determine the sand's mineral content in the Talang Siring tourist area in Pamekasan R

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Ahmed, Hussein M., Neama Ahmed Sobhy, Mohamed A. El-Khateeb, Mohammed M. Hefny, and Fatehy M. Abdel-Haleem. "Preparation and Characterization of Iron Nanoparticles by Green Synthesis Method and its Application in Water Treatment." Solid State Phenomena 342 (May 25, 2023): 11–25. http://dx.doi.org/10.4028/p-r1vxsa.

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The synthesized iron oxide nanoparticles by green synthesis method have been widely favored because of highly bio-degradable, ecofriendly, environmentally, low toxicity and highly reactive surfaces. The aim of this study, the magnetite iron nanoparticles (Fe/NPs) were preparing by waste natural materials such as banana, orange, and pomegranate peels, that’s consider as reducing agent. In this study, evaluate of the magnetite nanoparticles for removal of pollutants from wastewater, and determined of efficiency, yield, size, shape and morphology of the synthesized iron nanoparticle. The synthesi

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Bish, David, David Blake, David Vaniman, et al. "The first X-ray diffraction measurements on Mars." IUCrJ 1, no. 6 (2014): 514–22. http://dx.doi.org/10.1107/s2052252514021150.

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The Mars Science Laboratory landed in Gale crater on Mars in August 2012, and the Curiosity rover then began field studies on its drive toward Mount Sharp, a central peak made of ancient sediments. CheMin is one of ten instruments on or inside the rover, all designed to provide detailed information on the rocks, soils and atmosphere in this region. CheMin is a miniaturized X-ray diffraction/X-ray fluorescence (XRD/XRF) instrument that uses transmission geometry with an energy-discriminating CCD detector. CheMin uses onboard standards for XRD and XRF calibration, and beryl:quartz mixtures const

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Omar, Halo Dalshad. "The Analysis of Copper-Iron Metallic Mixture by Means of XRD and XRF." International Letters of Chemistry, Physics and Astronomy 64 (February 2016): 130–34. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.64.130.

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The objective of the paper has been given on observations based on studies of the three samples of copper-iron (Cu-Fe) alloy have been prepared from 3gm mass of copper of 99.9 % purity powder and adding 1gm weight of iron powder and adding 1.5gm weight of iron powder. A discussion about simple and low cost preparation of Cu-Fe alloy by Mini Mill 2 Panalytical and preparation of the sample was rotating at 10 min and in case of grinding samples at high speed 300 rpm. Herzog press Panalytical used to produce pressed powder Cu-Fe alloy. The characters of Cu-Fe particles are depending on their size

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Omar, Halo Dalshad. "The Analysis of Copper-Iron Metallic Mixture by Means of XRD and XRF." International Letters of Chemistry, Physics and Astronomy 64 (February 15, 2016): 130–34. http://dx.doi.org/10.56431/p-tj32k9.

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The objective of the paper has been given on observations based on studies of the three samples of copper-iron (Cu-Fe) alloy have been prepared from 3gm mass of copper of 99.9 % purity powder and adding 1gm weight of iron powder and adding 1.5gm weight of iron powder. A discussion about simple and low cost preparation of Cu-Fe alloy by Mini Mill 2 Panalytical and preparation of the sample was rotating at 10 min and in case of grinding samples at high speed 300 rpm. Herzog press Panalytical used to produce pressed powder Cu-Fe alloy. The characters of Cu-Fe particles are depending on their size

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Ahadova, Aybeniz, Ahmad Ahadov, Aqshin Abishov, Muslim Gurbanov, and Sahib Mammadov. "Firing conditions and production techniques of ancient ceramics." Journal of Radiation Researches 11, no. 1 (2024): 23–32. https://doi.org/10.5281/zenodo.14060132.

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During the firing process, the mineral components of ceramics experience phase transitions andchemical composition changes, and these processes depend on the temperature at which they are fired.Comprehensive analysis of ancient ceramics often involves the study of their mineralogical, chemical,and thermal characteristics. By analyzing the data through an interdisciplinary approach usingthermogravimetry (TG), thermoluminescence (TL), X-ray diffraction (XRD), and X-ray fluorescence(XRF) techniques and considering the archaeological context, researchers can draw important conclusionsabout the ori

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Schreiner, M., B. Frühmann, D. Jembrih-Simbürger, and R. Linke. "X-rays in art and archaeology: An overview." Powder Diffraction 19, no. 1 (2004): 3–11. http://dx.doi.org/10.1154/1.1649963.

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An overview of the techniques used in art and archaeology is presented and the applicability of X-ray radiography, X-ray fluorescence (XRF), and X-ray diffraction analysis (XRD) as a tool for nondestructive investigations of objects of art and archaeology is discussed. X-ray radiography, for example, is a standard technique widely used and accepted by art historians, archaeologists, curators, and conservators as this method enables information about the manufacturing process and the condition of an object without “touching” the artifact. XRF and XRD enable a nondestructive determination of the

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Reinhardt, Averie, Renfei Feng, Qunfeng Xiao, Yongfeng Hu та Tsun-Kong Sham. "Exploring the Dzi Bead with Synchrotron Light: XRD, XRF Imaging and μ-XANES Analysis". Heritage 3, № 3 (2020): 1035–45. http://dx.doi.org/10.3390/heritage3030056.

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The origin of Dzi beads, also called “tian zhu”, has always been a mystery. These beads come in a variety of patterns, shapes and sizes. They have cultural and heritage significance in Tibet and areas surrounding the Himalayas. The most recognized beads are those with the “eye” pattern. They are said to ward off evil spirits. Due to their reputation, the demand for Dzi beads has increased in Asia. Herein, we report a study of a Dzi bead with a three-eye pattern using X-ray diffraction (XRD), X-ray fluorescence (XRF), X-ray absorption near edge structure (XANES) and imaging techniques. This is

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Valadas, S., A. Candeias, J. Mirão та ін. "Study of Mural Paintings Using In Situ XRF, Confocal Synchrotron-μ-XRF, μ-XRD, Optical Microscopy, and SEM-EDS—The Case of the Frescoes from Misericordia Church of Odemira". Microscopy and Microanalysis 17, № 5 (2011): 702–9. http://dx.doi.org/10.1017/s1431927611000195.

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AbstractIn this work, we present the results of an analytical method developed for detailed pigment identification, stratigraphy, and degradation of the paint layers of mural paintings applied in the study of the 17th century frescoes from the Misericordia Church of Odemira (Southwest Portugal). In situ X-ray fluorescence spectrometry analyses were performed on three panels of the mural paintings and complemented by colorimetric measurements. The different color areas were also sampled as microfragments (approx. 1 mm2) that were studied as taken or mounted in epoxy resin to expose the differen

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Chayanun, Lert, Susanna Hammarberg, Hanna Dierks, et al. "Combining Nanofocused X-Rays with Electrical Measurements at the NanoMAX Beamline." Crystals 9, no. 8 (2019): 432. http://dx.doi.org/10.3390/cryst9080432.

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The advent of nanofocused X-ray beams has allowed the study of single nanocrystals and complete nanoscale devices in a nondestructive manner, using techniques such as scanning transmission X-ray microscopy (STXM), X-ray fluorescence (XRF) and X-ray diffraction (XRD). Further insight into semiconductor devices can be achieved by combining these techniques with simultaneous electrical measurements. Here, we present a system for electrical biasing and current measurement of single nanostructure devices, which has been developed for the NanoMAX beamline at the fourth-generation synchrotron, MAX IV

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Ngii, Edward, La Hamimu, Abdul Kadir, La Ode Hasan Jamilu, Adi Kumala, and Slamet Slamet. "Characterization of Substandard Limestone Aggregates Using XRF, XRD, and SEM: Implications for Cement Paste Reinforcement in Concrete Applications." MEDIA KONSTRUKSI 9, no. 4 (2024): 311–16. https://doi.org/10.33772/medkons.v9i4.79.

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This study investigates the properties of substandard limestone aggregates sourced from a quarry in Meleura Village, Muna Regency, Southeast Sulawesi, Indonesia, and explores their potential use in concrete applications. The aggregates were characterized using X-ray fluorescence (XRF), X-ray diffraction (XRD), and scanning electron microscopy (SEM) to assess their chemical composition, crystalline phases, and microstructural features. The XRF analysis revealed significant silica content, while XRD identified calcite, quartz, and dolomite as the primary phases. SEM analysis showed notable poros

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Bortolotti, M., L. Lutterotti, E. Borovin, and D. Martorelli. "Combined XRD-XRF cluster analysis for automatic chemical and crystallographic surface mappings." Powder Diffraction 34, S1 (2019): S36—S41. http://dx.doi.org/10.1017/s0885715619000216.

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X-ray diffraction-X-ray fluorescence (XRD-XRF) data sets obtained from surface scans of synthetic samples have been analysed by means of different data clustering algorithms, with the aim to propose a methodology for automatic crystallographic and chemical classification of surfaces. Three data clustering strategies have been evaluated, namely hierarchical, k-means, and density-based clustering; all of them have been applied to the distance matrix calculated from the single XRD and XRF data sets as well as the combined distance matrix. Classification performance is reported for each strategy b

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Mustafa, Rebaz M., Bashdar I. Meenaa, Emad K. Mohammed, et al. "Estimation of Minor and Trace Elements Concentration and Investigation of Chemical Composition of Kidney Stones in Kurdistan Region." Oriental Journal Of Chemistry 39, no. 2 (2023): 439–45. http://dx.doi.org/10.13005/ojc/390224.

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Investigations of the chemical composition of kidney stones are essential for understanding of the nature formation of stones and for the development of preventative treatment methods. Instrumental activation analysis radiations are significant tools for determining the composition of kidney stones. Kidney stones of varying compositions were investigated through the use of X-ray powder diffraction (XRD) and X-ray fluorescence (XRF) techniques. Materials can be observed in two very different ways due to the X-ray photon's unique interaction with matter. Using a combination of X-ray fluorescence

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Arboleda, Johana, and Adriana Echavarría. "X-ray powder diffraction data for two new compounds (NH4)1.5Ni2V2O7(OH)1.5 · H2O and (NH4)1.5Cu1.125Ni1.125V2O7(OH)2 · H2O." Powder Diffraction 26, S1 (2011): S51—S54. http://dx.doi.org/10.1154/1.3660817.

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Two new bimetallic and trimetallic compounds (NH4)1.5Ni2V2O7(OH)1.5 · H2O and (NH4)1.5Cu1.125 Ni1.125V2O7(OH)2 · H2O were synthesized by hydrothermal method and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and X-Ray fluorescence (XRF). Crystallographic studies showed that both compounds are hexagonal with space group P-62c.

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Ramli, Zuliskandar, Nik Hassan Shuhami Nik Abdul Rahman, Abdul Latif Samian, et al. "X-Ray Diffraction (XRD) and X-Ray Fluorescence (XRF) Analysis of Proto-historic Votive Tablets from Chawas Cave, Hulu Kelantan, Malaysia." Research Journal of Applied Sciences, Engineering and Technology 7, no. 7 (2014): 1381–87. http://dx.doi.org/10.19026/rjaset.7.405.

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Finkelshtein, Alexandr L., Roman V. Smely, Alena A. Amosova, and Victor M. Chubarov. "Estimation of the Biogenic Silica Content in Lacustrine Bottom Silicate Sediments by X-Ray Diffraction (XRD) and X-Ray Fluorescence (XRF)." Analytical Letters 55, no. 7 (2021): 1119–30. http://dx.doi.org/10.1080/00032719.2021.1988632.

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Xia, Jin Lan, Hong Chang Liu, Zhen Yuan Nie, et al. "Characterization of Microbe-Mineral Interfacial Interaction Based on Synchrotron Radiation Techniques." Advanced Materials Research 1130 (November 2015): 123–26. http://dx.doi.org/10.4028/www.scientific.net/amr.1130.123.

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This article presents the progress on characterization of the interfacial interaction between sulfur oxidizing microbes and sulfide minerals by using of synchrotron radiation-based techniques including S/Fe/Cu X-ray absorption near-edge structure spectroscopy (XANES), X-ray Diffraction (XRD), micro-X-ray fluorescence (μ-XRF) mapping and micro-scanning transmission X-ray microscopy (μ-STXM) imaging, together with other accessory approaches such as SEM/EDS, Raman spectroscopy, FT-IR spectroscopy, and electrochemical methods as well as comparative proteomics methodology.

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Dahani, Wiwik, Riskaviana Kurniawati, Rita Sundari, Irfan Marwanza, and Faisal Rachman. "PYROMETALLURGICAL PROCESS FOR ZINC ANALYSIS IN SPHALERITE APPLYING XRD AND XRF." Jurnal Rekayasa Mesin 15, no. 1 (2024): 411–24. http://dx.doi.org/10.21776/jrm.v15i1.1525.

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This paper has analyzed dominant zinc element in sphalerite naturally found together with galena in mineral ore. Since pyrometallurgical route related to roasting process is very common to mineral dressing, therefore, this investigation has studied the effect of varied roasting time (30 min, 60 min, and 90 min) and temperature (500oC, 600oC, and 700oC) on zinc mineral examination using XRD (X-Ray Diffraction) and zinc element using XRF (X-Ray Fluorescence) analyses. Previous studies usually applied cheaper AAS (Atomic Absorption Spectrometer) for zinc analysis in aqueous solution, however, sph

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Duangdee, Bheechanat, Dussadee Rattanaphra, Anusith Thanapimmetha, Maythee Saisriyoot, and Penjit Srinophakun. "Synthesis and Characterization of Mixed Rare Earths Hydroxide Catalyst." Materials Science Forum 936 (October 2018): 53–57. http://dx.doi.org/10.4028/www.scientific.net/msf.936.53.

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This work presents the synthesis and characterization of mixed rare earths hydroxide heterogeneous catalyst. The catalysts were prepared by co-precipitation of mixed rare earths with NaOH at different pH (6, 7 and 12). The prepared catalysts were characterized by X-ray fluorescence (XRF), X-ray diffraction (XRD) and scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM–EDS). The XRF results showed that the catalyst composed of cerium (Ce), neodymium (Nd), lanthanum (La), praseodymium (Pr) and samarium (Sm) being predominant at pH up to 7. Particularly, cerium (Ce) was fav

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รักไทยเจริญชีพ, ศันสนีย์, วราลี บางหลวง, เอมวจี ปานทอง та วรรณา ต.แสงจันทร์. "เคลือบเซรามิกจากเถ้าชานอ้อย". วารสารวิทยาศาสตร์ประยุกต์ กรมวิทยาศาสตร์บริการ 5, № 5 (2016): 31–38. http://dx.doi.org/10.60136/bas.v5.2016.279.

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เนื่องด้วยปริมาณเถ้าชานอ้อยในอุตสาหกรรมผลิตน้ำตาลเป็นวัสดุเหลือทิ้งที่มีจํานวนมาก ซึ่งนอกจากนําไปใช้ปรับปรุงดินแล้ว ยังไม่มีการนําไปใช้ประโยชน์อย่างอื่น การศึกษานี้มีวัตถุประสงค์เพื่อศึกษาความเป็นไปได้ในการใช้ประโยชน์จากเถ้าชานอ้อยเพื่อผลิตเคลือบเซรามิกโดยใช้วัตถุดิบหลัก 3 ชนิด ได้แก่ เถ้าชานอ้อย ดินดํา และแร่ฟันม้า จากผลวิเคราะห์องค์ประกอบทางเคมี (X-ray fluorescence : XRF) พบว่า เถ้าชานอ้อยมีองค์ประกอบหลัก คือ ซิลิกา ร้อยละ 71 อะลูมินา ร้อยละ 9 และ แคลเซียมออกไซด์ ร้อยละ 8 ผลวิเคราะห์องค์ประกอบทางแร่วิทยา (X-ray diffraction : XRD) พบเฟสหลักคือ ควอตซ์ กําหนดสูตรเคลือบโดยใช้วิธีแปรส่วนผสมในตารา

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Falkenberg, Gerald, Frank Seiboth, Frieder Koch, et al. "CRL optics and silicon drift detector for P06 Microprobe experiments at 35 keV." Powder Diffraction 35, S1 (2020): S34—S37. http://dx.doi.org/10.1017/s0885715620000536.

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A provisional setup for X-ray microprobe experiments at 35 keV is described. It is based on compound refractive lenses (CRLs) for nanofocusing and a Vortex silicon drift detector with 2 mm sensor thickness for increased sensitivity at high energies. The Microprobe experiment (PETRA III) generally uses Kirkpatrick-Baez mirrors for submicrometer focusing in the energy range of 5–21 keV. However, various types of scanning X-ray microscopy experiments require higher excitation energies. The CRL optics were characterized by X-ray ptychography and X-ray fluorescence (XRF) knife edge scans on a sieme

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Oloyede, Olukayode Gideon, Umar Omeiza Aroke, Saidat Olanipekun Giwa, and Alexander Asanja Jock. "Characterisation of Natural and HDTMA-Br Modified Dijah-Monkin Bentonite Clay: FTIR, XRF, XRD and SEM." Path of Science 7, no. 5 (2021): 2010–18. http://dx.doi.org/10.22178/pos.70-12.

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In this study, Dijah-Monkin bentonite clay was modified with a cationic surfactant hexadecyltrimethylammonium bromide (HDTMA-Br) at the level of twice the cation exchange capacity (CEC). This process results in the development of hydrophobic organoclay with an improved adsorption capacity. The clay obtained from Zing LGA Taraba State, North-East Nigeria, was beneficiated and pulverised to a particle size of 125 µm. The modification was performed without acid activation to prevent damages to the clay’s crystal structure. The organoclay was characterised for chemical composition, functional grou

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Piga, Giampaolo, Andrés Santos-Cubedo, Salvador Moya Solà, Antonio Brunetti, Assumpciò Malgosa, and Stefano Enzo. "An X-ray Diffraction (XRD) and X-ray Fluorescence (XRF) investigation in human and animal fossil bones from Holocene to Middle Triassic." Journal of Archaeological Science 36, no. 9 (2009): 1857–68. http://dx.doi.org/10.1016/j.jas.2009.04.013.

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Medeiros, Keila Machado, Vanessa Nóbrega Medeiros, Dayanne Diniz Souza Morais, Luana Rodrigues Kojuch, Edcleide Maria Araújo, and Hélio Lucena Lira. "Analysis of the Efficiency of Surface Treatment of Bentonite Clay for Application in Polymeric Membranes." Materials Science Forum 775-776 (January 2014): 493–97. http://dx.doi.org/10.4028/www.scientific.net/msf.775-776.493.

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The bentonite clay fillers are mostly used for the development of nanocomposites, due to having characteristics which provide to obtain in nanometric particles. The bentonite clay was treated with an ammonium quaternary salt to modify it to organophilic clay. The polymeric membranes and nanocomposites were prepared using the phase inversion technique. The bentonite and organophilic clays were characterized by X-ray fluorescence (XRF), X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR). The membranes were characterized by XRD. The results of XRF, XRD and FTIR confirmed t

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Siriprom, W., P. Kuha, S. Kongsriprapan, and K. Teanchai. "Studying Methylcellulose-Base Edible Films Properties by XRD, EDXRF and FTIR." Advanced Materials Research 979 (June 2014): 319–22. http://dx.doi.org/10.4028/www.scientific.net/amr.979.319.

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The physicochemical of methylcellulose (MC) base edible films were investigated in this work. The characterization of MC used X-Ray Diffraction (XRD), Energy Dispersive X-Ray Fluorescence (EDXRF) and Fourier Transform Infrared Spectroscopy (FTIR) spectroscopy for investigated the crystalline, the composition element, and the intermolecular interaction, respectively. It was found that, the XRD pattern indicated MC has amorphous structure. The chemical composition by XRF reported that Silver (Ag) have been detect and the hydrogen bonding formation between MC investigated with FTIR spectra, which

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Salim Jarjees, Qaidar, Abbas Rafaa Qasim, and Ammar Ahmed Hamdoon. "Synthesis and characterization of nickel and molybdenum catalysts supported on alumina derived from bauxite." Bulletin of the Chemical Society of Ethiopia 38, no. 6 (2024): 1715–24. http://dx.doi.org/10.4314/bcse.v38i6.17.

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In this study, a natural ore (bauxite), which is characterized by its high content of various aluminum minerals, such as gypsite, , bohmite, and diaspore, AlO(OH), was used to obtain alumina ( ), which was used as a support for the catalyst. The components of the ore were studied using multiple techniques, such as The X-ray energy dispersion (EDX) technique, X-ray diffraction (XRD) and X-ray fluorescence (XRF) technology. Then, undesirable components that negatively affect the behavior of the prepared catalyst were removed, such as carbonates, iron, and amorphous silica, and then aluminum oxid

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Medeiros, Keila Machado, Taciana Regina de Gouveia Silva, Luana Rodrigues Kojuch, Edcleide Maria Araújo, and Hélio Lucena Lira. "Preparation of Organoclay for Polymeric Nanocomposites Membranes." Materials Science Forum 727-728 (August 2012): 899–903. http://dx.doi.org/10.4028/www.scientific.net/msf.727-728.899.

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Bentonites are the most used fillers in the development of nanocomposites, due to their characteristics that provide nanosized particles, contributing to a large contact area between the clay and the polymer. In general, the additions of small amounts of organoclay improve the mechanical and thermal properties of nanocomposites. Bentonite clays and organoclays were characterized by X-ray fluorescence (XRF), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and thermogravimetry (TG). The results of XRF, XRD and FTIR confirmed the presence of quaternary ammonium salt in the

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Rakovan, John, Yun Luo, and Olaf Borkiewicz. "Synchrotron microanalytical methods in the study of trace and minor elements in apatite." Mineralogia 39, no. 1-2 (2008): 31–40. http://dx.doi.org/10.2478/v10002-008-0001-9.

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Synchrotron microanalytical methods in the study of trace and minor elements in apatiteSynchrotron X-ray facilities have the capability for numerous microanalytical methods with spatial resolutions in the micron to submicron range and sensitivities as low as ppm to ppb. These capabilities are the result of a high X-ray brilliance (many orders of magnitude greater than standard tube and rotating anode sources); a continuous, or white, spectrum through the hard X-ray region; high degrees of X-ray columniation and polarization; and new developments in X-ray focusing methods. The high photon flux

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Cappuccio, Giorgio, Giannantonio Cibin, Sultan Dabagov, et al. "Challenging X-ray Fluorescence Applications for Environmental Studies at XLab Frascati." Condensed Matter 3, no. 4 (2018): 33. http://dx.doi.org/10.3390/condmat3040033.

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In this work, we will report applications of the total external X-ray fluorescence (TXRF) station, a prototype assembled at the XLab Frascati laboratory (XlabF) at the INFN National Laboratories of Frascati (INFN LNF). XlabF has been established as a facility to study, design and develop X-ray optics, in particular, polycapillary lenses, as well as to perform X-ray experiments for both elemental analysis and tomography. The combination of low-power conventional sources and policapillary optics allows assembling a prototype that can provide a quasi-parallel intense beam for detailed X-ray spect

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Tian, Cai Juan, Rong Zhe Tang, Song Bai Hu, et al. "Comparative Studies of CdZnS Thin Films at Low Zinc Content Prepared by Vacuum Evaporation and CBD." Advanced Materials Research 225-226 (April 2011): 784–88. http://dx.doi.org/10.4028/www.scientific.net/amr.225-226.784.

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Cd1−xZnxS thin films at low Zn content were prepared both by chemical bath deposition (CBD) and vacuum co-evaporation. The X-ray fluorescence (XRF) and X-ray photoelectron spectroscopy (XPS) analysis were performed to determine the composition of the films, while the structural properties were investigated by X-ray diffraction (XRD). As a probable window layer, the optical band gaps of Cd1−xZnxS thin films prepared by the dry and wet process were calculated. Finally, the surface morphologies of the thin films were survey by scanning electron microscopy (SEM) and atomic force microscopy (AFM).

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Iordanidis, A., J. Garcia-Guinea, and G. Karamitrou-Mentessidi. "Characterisation of Mycenaean and matt-painted pottery from Alani, ancient upper Macedonia, Greece." Bulletin of the Geological Society of Greece 40, no. 4 (2007): 1796. http://dx.doi.org/10.12681/bgsg.17141.

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Several analytical methods were applied for the study of ancient pottery from Aiani, ancient upper Macedonia, northern Greece. Mycenaean and matt-painted pottery sherds, dated form Late Bronze age, were analysed with the help of X-Ray Diffraction (XRD), X-Ray Fluorescence (XRF) and Environmental Scanning Electron Microscopy, coupled with Energy Dispersive X-ray system (ESEM-EDX). Morphological, chemical and mineralogical characteristics of both types of ancient pottery indicated a rather local provenance, thus strengthening the hypothesis of the co-existence of Mycenaean and Dorian pottery wor

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Lv, Bin, Songbai Hu, Wei Li, et al. "Preparation and Characterization ofSb2Te3Thin Films by Coevaporation." International Journal of Photoenergy 2010 (2010): 1–4. http://dx.doi.org/10.1155/2010/476589.

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Deposition ofSb2Te3thin films on soda-lime glass substrates by coevaporation of Sb and Te is described in this paper.Sb2Te3thin films were characterized by x-ray diffraction (XRD), x-ray fluorescence (XRF), atomic force microscopy (AFM), x-ray photoelectron spectroscopy (XPS), electrical conductivity measurements, and Hall measurements. The abnormal electrical transport behavior occurred fromin situelectrical conductivity measurements. The results indicate that as-grownSb2Te3thin films are amorphous and undergo an amorphous-crystalline transition after annealing, and the posttreatment can effe

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Bukit, Nurdin, Erna Frida, Ferry Rahmat Astianta Bukit, and Bunga Fisikanta Bukit. "Analysis structure and morphology of bentonite-opba nanocomposites as nanofillers." Journal of Applied Research and Technology 20, no. 2 (2022): 117–25. http://dx.doi.org/10.22201/icat.24486736e.2022.20.2.1710.

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used as a nanofiller. The methods used to synthesis bentonite nanoparticles are ball mill and co-precipitation and modification with surfactant cetyltrimethylammonium bromide (CTAB). Likewise, the OPBA synthesis process with the ball mill process and co-precipitation. Characterization using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscope (SEM), FTIR and X-ray fluorescence (XRF). The results of characterization using XRD showed a decrease in particle size in bentonite-OPBA nanocomposites. The SEM results show uniformity of particle size in B

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Indriana, Rina Dwi, Hijrah Saputra, Mariyanto Mariyanto, Eleonora Agustin, Mimin Iryanti, and Cahyo Aji Hapsoro. "Rare Earth Element Characterization of Bledug Kuwu Mud Volcano, Central Java, Indonesia, based on Geochemical Analyzes (Susceptibility, XRF, XRD, SEM-EDS and ICP-EOS)." Sains Malaysiana 52, no. 9 (2023): 2529–43. http://dx.doi.org/10.17576/jsm-2023-5209-05.

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Mud volcano material is generally rich in oxides, while oxides are the main compounds forming rare earth elements. Bledug Kuwu, Central Java, Indonesia, is one of the active mud volcanoes, so there may be rare earth elements. This research is the characterization of rare earth elements (REE) in the Bledug Kuwu mud using magnetic and geochemical methods. Magnetic characterization uses magnetic susceptibility measurements. The geochemical characterization of the mud samples consisted of the XRF (X-Ray Fluorescence), XRD (X-Ray Diffraction), ICP-EOS (inductively coupled plasma) test, and the SEM-

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K.W, Shalbugau, Dass P.M, Iji M, Nkafamiya I. I, and Maitera O. N. "Development and characterization of catalyst materials from magnetic sand, Crotalaria pallida and kaolin." International Journal of Advanced Chemistry 9, no. 2 (2021): 188. http://dx.doi.org/10.14419/ijac.v9i2.31812.

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In this study, magnetic sand and Crotalaria pallida gotten from Adamawa and Bauchi states of Nigeria, respectively, were mixed after treatment, and impregnated with kaolin using a wet impregnation method and the resulting material was characterized using scanning electron microcopy (SEM), X-ray fluorescence (XRF) and X-ray diffraction (XRD). The result of XRF analysis revealed the existence of a number of dopant-like constituents in the sample, which substitute parts of important atoms in the spinel structure, however, not forming individual phases. The SEM micrographs displayed pore structure

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DISHONG, NINI HAVELA, AHMAD FADLY JUSOH, NASHA RODZIADI KHAW, et al. "INVESTIGATING THE GEOCHEMICAL CONTENT OF ANCIENT LATERITE BRICKS FROM BUKIT CHORAS ARCHAEOLOGICAL SITE USING X-RAY DIFFRACTION (XRD) AND X-RAY FLUORESCENCE (XRF)." JOURNAL OF SUSTAINABILITY SCIENCE AND MANAGEMENT 17, no. 1 (2022): 236–58. http://dx.doi.org/10.46754/jssm.2022.01.016.

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de Oliveira, Sara Verusca, Milena Costa da Silva, Gustavo Figueiredo Brito, Antônio Gilson Barbosa de Lima, and Edcleide Maria Araújo. "Influence of Bentonite Clay Content in HDPE Nanocomposites." Materials Science Forum 727-728 (August 2012): 1780–84. http://dx.doi.org/10.4028/www.scientific.net/msf.727-728.1780.

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This research is to obtain nanocomposites of HDPE/bentonite clay. Inorganic polymers reinforced with materials are of great interest due to their applications in automotive, and electrical and electronic industries. The nanocomposites were produced by melt intercalation with different percentages of clay and compared with pure HDPE. Clay was used as modified and unmodified and it was characterized by X-ray diffraction (XRD) and X-ray fluorescence (XRF). The obtained nanocomposites were characterized through thermogravimetry (TG). It was verified by XRF that clay performed compositions of bento

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Sedlačková, Katarína, Jozef Sitek, Patrik Novák, and Július Dekan. "Analysis of Mount Etna’s volcanic rocks." Journal of Electrical Engineering 72, no. 2 (2021): 106–12. http://dx.doi.org/10.2478/jee-2021-0014.

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Abstract In this work we have analysed the basalt rocks from the area of Mount Etna using 57Fe Mössbauer spectroscopy (MS), X-ray diffraction (XRD) and X-ray fluorescence analysis (XRF). Mössbauer spectroscopy was used to identify and to quantify the content and the magnetic nature of the iron-bearing minerals in the lava samples. Magnetite, olivine, pyroxene, hornblende, hematite and goethite of different relative abundances were found in the investigated samples. X-ray diffraction supported the structural analysis and determined the phases not visible by MS, like albite and calcite. X-ray fl

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Mutiso, Selline, Keisuke Nakayama, and Katsuaki Komai. "A Simple Neural Network for Estimating Fine Sediment Sources Using XRF and XRD." Hydrology 11, no. 11 (2024): 192. http://dx.doi.org/10.3390/hydrology11110192.

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Suspended sediment (SS) has a wide range of negative effects such as increased water turbidity, altered habitat structures, sedimentation, and effects on hydraulic systems and environmental engineering projects. Nevertheless, the methods for accurately determining SS sources on a basin-scale are poorly understood. Herein, we used a simplified neural network analysis (NNA) model to identify the sources of SS in Japan’s Oromushi River Catchment Basin. Fine soil samples were collected from different locations of the catchment basin, processed, and separately analysed using X-ray fluorescence (XRF

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