Academic literature on the topic 'XXXXIX'

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Journal articles on the topic "XXXXIX"

1

Protiva, Miroslav, Jiří Jílek, Miroslav Rajšner, et al. "Fluorinated tricyclic neuroleptics with prolonged action: derivatives and analogues of 2-(4-(7-fluoro-2-isopropyl-10,11-dihydrodibenzo[b,f]thiepin-11-yl)-piperazine-1-yl)ethanol." Collection of Czechoslovak Chemical Communications 52, no. 7 (1987): 1811–33. http://dx.doi.org/10.1135/cccc19871811.

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The preparation of 4-fluoro-2-nitrobenzonitrile (V), an intermediate in the synthesis of the title compound I, from 4-fluoro-2-nitroaniline via 5-fluoro-2-iodonitrobenzene (VII) was elaborated. Syntheses of 1,1,1,3,3,3-hexadeutero-2-propyl (XX) and 1,3,4-trideutero (XXVIII) analogues of compound I from hexadeuteroacetone, and pentadeuterobromobenzene, respectively, were carried out. Compound I was esterified with acetic anhydride, decanoic acid and 3,4,5-trimethoxybenzoyl chloride to give the esters II-IV. Acylation of compound XXX with acetyl chloride, 4-fluorophenoxyacetyl chloride and (4-fl
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2

Pouzar, Vladimír, Hana Chodounská, Dalibor Sameš, Pavel Drašar та Miroslav Havel. "Derivatives of 5α-androstan-3α- and 3β-ol with acrylate side chain". Collection of Czechoslovak Chemical Communications 55, № 5 (1990): 1243–56. http://dx.doi.org/10.1135/cccc19901243.

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Hydroxy derivatives I, II, III, XVII and XX were oxidized to give the respective aldehydes IV, V, VI, XVIII and XXI which were further converted by Wittig-Horner reaction into unsaturated methyl and ethyl esters. Removal of the acetal protecting group in position 3 afforded methylesters X, XXIV and XXXVI and ethyl esters XIV, XXV and XXXVII. Compounds XXIV, XXV, XXXVI and XXXVII were converted into the corresponding hemisuccinates XXVIII, XXIX, XL and XLI and β-D-glucosides XXXII, XXXIII, XLIV and XLV.
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3

Hulinská, Hana, Miroslav Ryska, Ivan Koruna, et al. "Some further 2-(4-substituted 1-piperazinyl)acetamides derived from 6,11-dihydrodibenzo[b,e]thiepin. Transformations of 6,11-dihydrodibenzo[b,e]thiepin derivatives into anthraquinones, anthrones and anthracenes." Collection of Czechoslovak Chemical Communications 54, no. 5 (1989): 1388–402. http://dx.doi.org/10.1135/cccc19891388.

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Reactions of the secondary amines I and VIII with chloroacetyl chloride gave the 2-chloroacetamides II and IX affording by substitution reactions with 1-methylpiperazine, 2-(1-piperazinyl)ethanol and 3-(1-piperazinyl)propanol in the title compounds III-V and X-XII. The starting amine VIII was prepared from the ketone XIV via XVII and VII. The product of 1,6-addition and the following dehydrogenation XVIII was obtained as a by-product of the reaction of XIV with 1-methyl-4-piperidylmagnesium chloride. Reaction of 2-fluorodibenzo[b,e]thiepin-11(6H)-one (XV) with sodium hydride in dimethylformami
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4

Jindřich, Jindřich, Hana Dvořáková, and Antonín Holý. "Synthesis of Isomeric N-(3-Fluoro-2-hydroxypropyl) and N-(2-Fluoro-3-hydroxypropyl) Derivatives of Purine and Pyrimidine Bases." Collection of Czechoslovak Chemical Communications 57, no. 7 (1992): 1466–82. http://dx.doi.org/10.1135/cccc19921466.

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Reaction of fluoromethyloxirane (III) with heterocyclic bases in the presence of potassium carbonate afforded N-(3-fluoro-2-hydroxypropyl) derivatives of adenine (VI), 3-deazaadenine (VII), 2-amino-6-chloropurine (XII), 6-nitro-1-deazapurine (IX), 4-methoxy-2-pyrimidone (XVIII) and its 5-methyl derivative (XIX). Acid hydrolysis of compounds XII, XVIII, and XIX gave 9-(3-fluoro-2-hydroxypropyl)guanine (XIII), 1-(3-fluoro-2-hydroxypropyl)uracil (XX) and -thymine (XXI). The intermediates XVIII and XIX were ammonolyzed to give 1-(3-fluoro-2-hydroxypropyl)cytosine (XXII) and -5-methylcytosine (XXII
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5

Machtoub, G. El. "Channel-specific dielectronic recombination of Ge(XXXII), Se(XXXIV), and Kr(XXXVI)." Canadian Journal of Physics 82, no. 4 (2004): 277–89. http://dx.doi.org/10.1139/p04-011.

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We present explicit calculations of channel-specific dielectronic recombination cross sections for hydrogen-like germanium, Ge(XXXII); selenium, Se(XXXIV); and krypton, Kr(XXXVI). The convoluted cross sections characterize K-shell emission spectra over a wide energy range where contributions from high-n (n = 2–10), satellite lines are included. The high-n contributions presented are important for better diagnostics in the domain of high-temperature plasmas. PACS Nos.: 32.30.Rj, 32.70.Rm, 34.70.te
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6

Bernardo-Filho, Mario. "Editorial." Brazilian Journal of Health and Biomedical Sciences 20, no. 1 (2021): 10. http://dx.doi.org/10.12957/bjhbs.2021.59720.

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7

Doschek, G. A., W. E. Behring, M. C. Richardson, et al. "Spectra and energy levels of Sm xxxiv, Eu xxxv, Gd xxxvi, and yb xxxxii." Journal of the Optical Society of America B 5, no. 2 (1988): 243. http://dx.doi.org/10.1364/josab.5.000243.

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8

Cherry, Joanna. "S. A. Bennett, PERSONAL INJURY DAMAGES IN SCOTLAND Edinburgh: Barnestoneworth Press, 1999. xxxxix and 453 pp (incl index). ISBN 0 9534152 0 1. £100." Edinburgh Law Review 4, no. 3 (2000): 359–60. http://dx.doi.org/10.3366/elr.2000.4.3.359.

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9

Dvořáková, Hana, Antonín Holý, Ivan Votruba, and Milena Masojídková. "Synthesis and Biological Effects of Acyclic Analogs of Deazapurine Nucleosides." Collection of Czechoslovak Chemical Communications 58, no. 3 (1993): 629–48. http://dx.doi.org/10.1135/cccc19930629.

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Deaza analogs of three basic types of S-adenosyl-L-homocysteine hydrolase (SAHase) inhibitors, (S)-DHPA (I), eritadenine (II) and AHPA (III), were prepared. Alkylation of 3-deazaadenine (V), 3-deazapurine (VI), 1-deazaadenine (VII) and 4-amino-6-bromo-5-cyanopyrrolo[2,3-d]pyrimidine (XXII) with (R)-2,2-dimethyl-4-tosyloxymethyl-1,3-dioxolane (XIIIb), followed by acid hydrolysis, afforded the corresponding (S)-2,3-dihydroxypropyl derivatives XVIIa -XIXa and XXV. Reaction of V and VII with 2,3-O-cyclohexylidene-D-erythrono lactone (XXIX) and subsequent removal of the protecting groups in an acid
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10

Polman, Jiří, та Alexander Kasal. "The synthesis of 5-methyl-19-nor-5β-pregna-9,16-diene-3,20-dione, 5-methyl-19-nor-5β-pregna-9,10-diene-3,6,20-trione and their analogues with annellated E ring". Collection of Czechoslovak Chemical Communications 56, № 12 (1991): 2892–905. http://dx.doi.org/10.1135/cccc19912892.

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The synthesis of compounds VII, XVII, XXXIV and XXXVII is described, in which biological activity is assumed. The key steps of their preparation are the dehalogenation of compound XVIII and radicalic deoxygenation of the 6β-hydroxy group in compound XXX, which take place without skeletal rearrangements.
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