Academic literature on the topic 'Zinc borate synthesis'

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Journal articles on the topic "Zinc borate synthesis"

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Kozerozhets, Irina V., Varvara V. Avdeeva, Grigorii A. Buzanov, Evgeniy A. Semenov, Yulia V. Ioni, and Sergey P. Gubin. "A New Approach for the Synthesis of Powder Zinc Oxide and Zinc Borates with Desired Properties." Inorganics 10, no. 11 (2022): 212. http://dx.doi.org/10.3390/inorganics10110212.

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Zinc borates are widely used in industry due to their thermal stability as a flame retardant in the production of plastics, rubber, and other polymer compositions. We have developed a simple and effective approach for the synthesis of zinc borate powders with desired properties, including desired particle size, low bulk density, high reactivity, etc. Zinc borates were prepared by the thermal treatment of a concentrated water–carbohydrate solution of a zinc salt until finely dispersed ZnO was formed, followed by its hydrothermal treatment at 90–300 °C as part of a suspension based on a hot aque
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Ersan, Ali Can, Azmi Seyhun Kipcak, Meral Yildirim Ozen, and Nurcan Tugrul. "An accelerated and effective synthesis of zinc borate from zinc sulfate using sonochemistry." Main Group Metal Chemistry 43, no. 1 (2020): 7–14. http://dx.doi.org/10.1515/mgmc-2020-0002.

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AbstractRecently, sonochemistry has been used for the synthesis of inorganic compounds, such as zinc borates. In this study using zinc sulphate heptahydrate (ZnSO4·7H2O) and boric acid (H3BO3) as starting materials, a zinc borate compound in the form of Zn3B6O12·3.5H2O was synthesized using an ultrasonic probe. Product’s characterization was carried out with using X-ray diffraction (XRD), Scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FT-IR) and Raman spectroscopy. Zinc borate compound’s chemical bond structure was observed with Raman and FTIR. From the XRD result
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Gao, Pingqiang, and Yan Zhang. "Synthesis and Characterization of Zinc Borate Nanowhiskers and Their Inflaming Retarding Effect in Polystyrene." Journal of Nanomaterials 2015 (2015): 1–6. http://dx.doi.org/10.1155/2015/925060.

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Zinc borate nanowhiskers 4ZnO·B2O3·H2O were in situ successfully synthesized via one-step precipitation reaction. A set of experiments was performed to evaluate the influence of reaction temperature. Increasing the temperature up to 70°C led to the high purity of zinc borate nanowhiskers with a monoclinic crystal structure measuring 50 nm to 100 nm in diameter and approximately 1 µm in length. However, higher temperature decreases the crystallization due to the emergence of other styles of zinc borate. Flame-resistant nanocomposites of polystyrene and zinc borate nanowhiskers were also success
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Fatma Tugce Senberber Dumanli, Fatma Tugce Senberber Dumanli, Azmi Seyhun Kipcak Azmi Seyhun Kipcak, and Duygu Sena Vardar and Nurcan Tugrul Duygu Sena Vardar and Nurcan Tugrul. "Ultrasonic-Assisted Synthesis of Zinc Borates: Effect of Boron Sources." Journal of the chemical society of pakistan 42, no. 6 (2020): 839. http://dx.doi.org/10.52568/000703.

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Sonochemistry meaning ultrasound-assisted chemistry plays an important role in the synthesis of inorganic compounds. Among these inorganic compounds, zinc borates are used for the flame-retarding agent. In this study using zinc chloride (ZnCl2), boric acid (H3BO3), Na2B4O7and#183;10H2O, Na2B4O7and#183;5H2O and NaOH as raw materials, a zinc borate compound in the formulae of Zn3B6O12and#183;3.5H2O was obtained using an ultrasonic probe. Crystal structures of samples were identified using X-ray diffraction (XRD). The symmetric and asymmetric stretching between boron and oxygen atoms were searche
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Fatma Tugce Senberber Dumanli, Fatma Tugce Senberber Dumanli, Azmi Seyhun Kipcak Azmi Seyhun Kipcak, and Duygu Sena Vardar and Nurcan Tugrul Duygu Sena Vardar and Nurcan Tugrul. "Ultrasonic-Assisted Synthesis of Zinc Borates: Effect of Boron Sources." Journal of the chemical society of pakistan 42, no. 6 (2020): 839. http://dx.doi.org/10.52568/000703/jcsp/42.06.2020.

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Sonochemistry meaning ultrasound-assisted chemistry plays an important role in the synthesis of inorganic compounds. Among these inorganic compounds, zinc borates are used for the flame-retarding agent. In this study using zinc chloride (ZnCl2), boric acid (H3BO3), Na2B4O7and#183;10H2O, Na2B4O7and#183;5H2O and NaOH as raw materials, a zinc borate compound in the formulae of Zn3B6O12and#183;3.5H2O was obtained using an ultrasonic probe. Crystal structures of samples were identified using X-ray diffraction (XRD). The symmetric and asymmetric stretching between boron and oxygen atoms were searche
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Sultygova, Z. Kh, L. I. Kitieva, and Timur A. Borukaev. "Using Zinc Borate as Effective Flame Retardant." Key Engineering Materials 816 (August 2019): 129–33. http://dx.doi.org/10.4028/www.scientific.net/kem.816.129.

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A directed synthesis of zinc borate was carried out in order to obtain a product with a specific chemical composition and specified characteristics, which was used as a flame retardant for the polymer. It was found that the introduction of the obtained zinc borate into high-density polyethylene leads to a significant increase in the fire resistance of the starting polymer. It is shown that the deformation-strength properties of high-density polyethylene do not deteriorate with the introduction of zinc borate, but remain at the level of the original polymer.
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Liu, Xin, Shao Ju Bian, Dan Dan Gao, Qing Fen Meng, Ming Wei, and Wu Li. "The Synthesis and Characterization of Zinc Borate Zn2B6O11·7H2O." Advanced Materials Research 652-654 (January 2013): 795–98. http://dx.doi.org/10.4028/www.scientific.net/amr.652-654.795.

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Zinc borate Zn2B6O11•7H2O was prepared at room temperature using Na2B4O7•10H2O, ZnSO4•7H2O and H3BO3 as raw materials. The synthesized product was characterized by XRD, SEM, TG-DSC and FT-IR. SEM results showed that the synthesized zinc borate had uniform morphology with a length up to a few microns. The experiment result indicates that additional H3BO3 in starting materials was beneficial to the uniform morphology of Zn2B6O11•7H2O.
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Tian, Yumei, Yupeng Guo, Man Jiang, et al. "Synthesis of hydrophobic zinc borate nanodiscs for lubrication." Materials Letters 60, no. 20 (2006): 2511–15. http://dx.doi.org/10.1016/j.matlet.2006.01.108.

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Ting, Chen, Deng Jian-Cheng, Wang Long-Shuo, Yang Fan, and Feng Gang. "Synthesis of a new netlike nano zinc borate." Materials Letters 62, no. 14 (2008): 2057–59. http://dx.doi.org/10.1016/j.matlet.2007.11.015.

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Zheng, Yunhui, Yumei Tian, Honglei Ma, et al. "Synthesis and performance study of zinc borate nanowhiskers." Colloids and Surfaces A: Physicochemical and Engineering Aspects 339, no. 1-3 (2009): 178–84. http://dx.doi.org/10.1016/j.colsurfa.2009.02.018.

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Dissertations / Theses on the topic "Zinc borate synthesis"

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Yao, Zhao Yue. "Synthesis, structure, and mechanical properties of lead- and zinc-copper borate glasses." Thesis, Rennes 1, 2016. http://www.theses.fr/2016REN1S080.

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Le but de ce travail est d'étudier l'effet de la teneur en cuivre et de la valence des atomes de cuivre sur la structure et les propriétés mécanique du verre. Des verres de zinc- et plomb- cuivre borate ont été étudiés. Les changements structurels avec le remplacement de PbO ou ZnO par CuO sont observés par réflectance infrarouge et Raman. L'état d'oxydation, l'environnement du site et la liaison caractéristique d'ions de cuivre ont été étudiés par spectroscopie optique et de résonance de spin électronique. Les propriétés mécaniques ont été déterminées et corrélées à la structure du verre et à
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Baltaci, Berk. "Sytnhesis And Characterization Of Nano Zinc Borate And Its Usage As A Flame Retardant For Polymers." Master's thesis, METU, 2010. http://etd.lib.metu.edu.tr/upload/12612701/index.pdf.

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The objectives of this study are to synthesize sub-micron sized zinc borate and to use them with other flame retardant additives in poly(ethylene terephthalate) (PET) based composites. The study can be divided into two parts. In the first part, it was aimed to synthesize sub-micron sized zinc borate (2ZnO.3B2O3.3.5H2O) with the reaction of zinc oxide and boric acid. For this purpose, low molecular weight additives or surfactants were used in the syntheses to prevent the agglomeration and to decrease particle size. Effect of type of surfactant and its concentration<br>effect of using nano-sized
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Paul, Avijit Kumar. "New Anions In The Assembly Of The Open-Framework Compounds : Synthesis, Structure And Properties." Thesis, 2010. https://etd.iisc.ac.in/handle/2005/1928.

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Open-framework inorganic materials constitute an important area of study in materials chemistry, because of their potential applications in areas such as sorption and catalysis. After the discovery of nanoporous aluminium phosphates (AlPOs) by Flanigen et al in 1982, there has been a tremendous growth in the area of porous solids that are based on phosphates. Apart from phosphates, phosphites, arsenates, sulfates, sulfites, selenates, selenites etc. have also been investigated. In addition to the different anions, the framework compounds now encompass almost all the elements of the periodic t
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Paul, Avijit Kumar. "New Anions In The Assembly Of The Open-Framework Compounds : Synthesis, Structure And Properties." Thesis, 2010. http://hdl.handle.net/2005/1928.

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Open-framework inorganic materials constitute an important area of study in materials chemistry, because of their potential applications in areas such as sorption and catalysis. After the discovery of nanoporous aluminium phosphates (AlPOs) by Flanigen et al in 1982, there has been a tremendous growth in the area of porous solids that are based on phosphates. Apart from phosphates, phosphites, arsenates, sulfates, sulfites, selenates, selenites etc. have also been investigated. In addition to the different anions, the framework compounds now encompass almost all the elements of the periodic t
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Book chapters on the topic "Zinc borate synthesis"

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Taber, Douglass F. "Carbon-Carbon Bond Formation." In Organic Synthesis. Oxford University Press, 2013. http://dx.doi.org/10.1093/oso/9780199965724.003.0025.

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Akiya Ogawa of Osaka Prefecture University found (Tetrahedron Lett. 2010, 51, 6580) that the Sm-mediated reductive coupling of a halide 1 with CO2 to give the carboxylic acid 2 was strongly promoted by visible light. Gregory C. Fu of MIT designed (Angew. Chem. Int. Ed. 2010, 49, 6676) a Ni catalyst for the coupling of a primary borane 4 with a secondary alkyl halide 3. James P. Morken of Boston College devised (Org. Lett. 2010, 12, 3760) conditions for the carbonylative conjugate addition of a dialkyl zinc to an enone 6 to give the 1,4-dicarbonyl product 7. Louis Fensterbank of the Institut Pa
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Taber, Douglass F. "Best Synthetic Methods: Oxidation and Reduction." In Organic Synthesis. Oxford University Press, 2013. http://dx.doi.org/10.1093/oso/9780199965724.003.0010.

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Johannes G. de Vries of DSM Pharmaceuticals prepared (Chem. Commun. 2009, 3747) Fe nanoparticles that selectively mediated the hydrogenation of Z alkenes and not trisubstituted alkenes. This should allow the conversion of 1 to 2. In the course of a synthesis (Tetrahedron Lett. 2009, 50, 4368) of centrolobine, Teck-Peng Loh of Nanyang Technological University employed an elegant protocol for the reduction of the secondary bromide 3. István Markó of the Université catholique de Louvain observed (Tetrahedron 2009, 65, 10930) that toluates such as 5 can be reduced smoothly with SmI2 to the corresp
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Taber, Douglass F. "C–N Ring Construction: The Waser Synthesis of Jerantinine E." In Organic Synthesis. Oxford University Press, 2017. http://dx.doi.org/10.1093/oso/9780190646165.003.0053.

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James A. Bull of Imperial College London prepared (J. Org. Chem. 2013, 78, 6632) the aziridine 2 with high diastereocontrol by adding the anion of diiodomethane to the imine 1. Karl Anker Jørgensen of Aarhus University observed (Chem. Commun. 2013, 49, 6382) high ee in the distal aziridination of 3 to give 4. Benito Alcaide of the Universidad Complutense de Madrid and Pedro Almendros of ICOQ- CSIC Madrid reduced (Adv. Synth. Catal. 2013, 355, 2089) the β-lactam 5 to the azetidine 6. Hiroaki Sasai of Osaka University added (Org. Lett. 2013, 15, 4142) the allenoate 8 to the imine 7, delivering t
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Conference papers on the topic "Zinc borate synthesis"

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Gao, Pingqiang, Wenhua Song, Feng Ding, and Xing Wang. "Synthesis of a new lamellar nano zinc borate." In 2013 International Conference on Materials for Renewable Energy and Environment (ICMREE). IEEE, 2013. http://dx.doi.org/10.1109/icmree.2013.6893742.

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Subhashini, Soumalya Bhattacharya, H. D. Shashikala, and N. K. Udayashankar. "Synthesis and studies on microhardness of alkali zinc borate glasses." In SOLID STATE PHYSICS: Proceedings of the 58th DAE Solid State Physics Symposium 2013. AIP Publishing LLC, 2014. http://dx.doi.org/10.1063/1.4872742.

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Mahajan, Rubby, Sandeep Kumar, Ram Prakash, and Vinay Kumar. "Synthesis and luminescent properties of Sm3+ activated lithium zinc borate phosphor." In NATIONAL CONFERENCE ON RECENT ADVANCES IN EXPERIMENTAL AND THEORETICAL PHYSICS (RAETP-2018). Author(s), 2018. http://dx.doi.org/10.1063/1.5051301.

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