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Journal articles on the topic 'Bromosuccinimide'

Author: Grafiati

Published: 4 June 2021

Last updated: 28 July 2025

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1

OIZUMI, Mitsuru. "N-Bromosuccinimide." Journal of Synthetic Organic Chemistry, Japan 51, no. 1 (1993): 68–69. http://dx.doi.org/10.5059/yukigoseikyokaishi.51.68.

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2

Mavračić, Juraj, Dominik Cinčić, and Branko Kaitner. "Halogen bonding ofN-bromosuccinimide by grinding." CrystEngComm 18, no. 19 (2016): 3343–46. http://dx.doi.org/10.1039/c6ce00638h.

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Two halogen bonded cocrystals ofN-bromosuccinimide and 4,4′-bipyridine, with stoichiometric ratios 1 : 1 and 2 : 1, have been synthesized and characterized. We present the first mechanochemical cocrystallization ofN-bromosuccinimide.

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3

Andin, A. N., and M. A. Engelgardt. "Synthesis of Functionalized Spiro[1-benzofuran-2,5'-pyrimidine] Derivatives of 5-Arylidenebarbituric Acids." Russian Journal of Organic Chemistry 60, no. 11 (2024): 2125–29. https://doi.org/10.1134/s1070428024110058.

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Abstract Adducts of dimedone and 5-arylidenebarbituric acids react with N-bromosuccinimide in aqueous ethanol to give functionalized spiro[1-benzofuran-2,5'-pyrimidine] derivatives with moderate yields. The reaction of 5-benzylidenebarbituric acid with ethyl acetoacetate in the presence of N-bromosuccinimide provides spiro[pyrimidine-5,6'-furo[2,3-d]pyrimidine].

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4

Ghassemzadeh, Mitra, Klaus Harms, Kurt Dehnicke та Dieter Fenske. "μ2-Halogenokomplexe von N-Bromsuccinimid und N-Bromphthalimid. Die Kristallstrukturen von PPh4[X(N-Bromsuccinimid)2] und von PPh4[X(N-Bromphthalimid)2] mit X = CI und Br / μ2-Halogeno Complexes of N-Bromosuccinimide and N-Bromophthalimide. The Crystal Structures of PPh4 [X(N-Bromosuccinimide)2] and PPh4 [X(N-Brom ophthalimide)2] with X = Cl and Br". Zeitschrift für Naturforschung B 49, № 5 (1994): 593–601. http://dx.doi.org/10.1515/znb-1994-0504.

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The μ2-halogeno complexes PPh4[X(N-bromosuccinimide)2] and PPh4[X(N-bromophthali- mide)2] with X = Cl and Br have been prepared by reactions of N-bromosuccinimide and N-bromophthalimide, respectively, with the corresponding tetraphenylphosphonium halides PPh4X in acetonitrile solutions. The compounds form pale yellow crystal needles, which were characterized by IR spectroscopy and by crystal structure determinations. PPh4[Cl(N-Bromosuccinimide)2] (1): Space group P21/n, Z = 4, structure solution with 2516 observed unique reflections, R = 0.040. Lattice dimensions at -25 °C: a = 1775.9(1), b =

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5

Singh, Minu. "Kinetic Treatment of the Reaction of Fructose and N-Bromosuccinimide in Cationic/Anionic/Nonionic Micelles." Journal of Soft Matter 2014 (September 30, 2014): 1–10. http://dx.doi.org/10.1155/2014/791563.

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The kinetics of oxidation of fructose by N-bromosuccinimide in acidic medium in the absence and presence of cationic, anionic, and nonionic surfactants has been measured iodometrically under pseudo-first-order condition. The oxidation kinetics of fructose by N-bromosuccinimide shows a first-order dependence on N-bromosuccinimide, fractional order dependence on fructose, and negative fractional order dependence on sulfuric acid. The kinetics is treated using Berezin’s micellar model that was previously used for the catalysis and inhibition of the reaction. The determined stoichiometric ratio wa

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6

Bera, Smritilekha, Dhananjoy Mondal, and Bhaskar Chatterjee. "Application of N-Bromosuccinimide in Carbohydrate Chemistry." SynOpen 07, no. 04 (2023): 501–10. http://dx.doi.org/10.1055/s-0042-1751501.

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AbstractThis article describes the use of N-bromosuccinimide in different organic group transformations in carbohydrate chemistry. A comprehensive discussion on the synthesis of deoxysugars through selective O-benzylidene fragmentation, photobromination, halogenation, oxidation, and polymerisation of different carbohydrate moieties with the aid of N-bromosuccinimide (NBS) is presented. The use of NBS in the most significant glycosylation methods and in oligosaccharide synthesis is also discussed.

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7

Sanad, H. M., and Alhussein A. Ibrahim. "Radioiodination, diagnostic nuclear imaging and bioevaluation of olmesartan as a tracer for cardiac imaging." Radiochimica Acta 106, no. 10 (2018): 843–50. http://dx.doi.org/10.1515/ract-2018-2960.

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Abstract The present work has been oriented to prepare radioiodinated olmesartan for a potential cardiac imaging. Olmesartan has been labeled using 125I or 131I with N-bromosuccinimide (NBS) as an oxidizing agent. Many factors like amount of N-bromosuccinimide, amount of substrate, pH, reaction temperature and reaction time, have been systematically studied to optimize high yield of [125I]iodoolmesartan. The biological distribution indicates the suitability of [125I]iodoolmesartan as a novel tracer to image heart.

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8

Khazaei, Ardeshir, Amin Rostami, Ayeh Raiatzadeh, and Marjan Mahboubifar. "N-Bromosuccinimide (NBS) — Selective and effective catalyst for trimethylsilylation of alcohols and phenols using hexamethyldisilazane and their regeneration under mild and neutral reaction conditions." Canadian Journal of Chemistry 85, no. 5 (2007): 336–40. http://dx.doi.org/10.1139/v07-029.

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Structurally diverse alcohols and phenols were trimethylsilylated in a clean and efficient reaction with hexamethyldisilazane (HMDS) based on the use of a catalytic amount of N-bromosuccinimide under both dichloromethane and solvent-free conditions at room temperature. Deprotection of trimethylsilyl ethers was also be achieved efficiently in the presence of a catalytic amount of NBS in methanol at ambient temperature.Key words: N-bromosuccinimide, solvent-free, alcohols, phenols, hexamethyldisilazane, trimethylsilyl ether, catalyst, detrimethylsilylation.

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9

Giridhar Reddy, P., K. Ramesh, S. Shylaja, K. C. Rajanna, and S. Kandlikar. "Ru (III) Catalyzed Oxidation of Aliphatic Ketones by N-Bromosuccinimide in Aqueous Acetic Acid: A Kinetic Study." Scientific World Journal 2012 (2012): 1–7. http://dx.doi.org/10.1100/2012/456516.

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Kinetics of Ru (III) catalyzed oxidation of aliphatic ketones such as acetone, ethyl methyl ketone, diethyl ketone, iso-butylmethyl ketone by N-bromosuccinimide in the presence of Hg(II) acetate have been studied in aqueous acid medium. The order of [N-bromosuccinimide] was found to be zero both in catalyzed as well as uncatalyzed reactions. However, the order of [ketone] changed from unity to a fractional one in the presence of Ru (III). On the basis of kinetic features, the probable mechanisms are discussed and individual rate parameters evaluated.

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10

Salman, Noori Y. "Kinetics Study of the Reaction between Serine and N-Bromosuccinimide in the Presence of Palladium (Pd2+)." INTERNATIONAL JOURNAL OF DRUG DELIVERY TECHNOLOGY 12, no. 02 (2022): 771–74. http://dx.doi.org/10.25258/ijddt.12.2.54.

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The oxidation of serine using N-bromosuccinimide (NBS) has been studied at fix pH value. The reaction presents a first-order reaction with respect to both substrate and oxidant. It is noted that the rate of reaction increases with increasing the palladium ion concentration. The addition of the reaction product (succinimide) affects the oxidation reaction rate. The protonated Br+ or NBrS and NBrS are used to be the reactive species of the N-bromosuccinimide. Furthermore, intermediate compounds are noticed through the reaction. Finally, a mechanism for the oxidation reaction is suggested in this

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11

Yamuna Princy S and Vidyavati shastry. "Mechanism and Kinetics Studies of Oxidation of the Pharmaceutical Drug Amlodipine Besylate by N-bromosuccinimide in Aqueous Acidic Medium." International Journal of Research in Pharmaceutical Sciences 11, SPL4 (2020): 1415–22. http://dx.doi.org/10.26452/ijrps.v11ispl4.4315.

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The oxidation of the pharmaceutical drug Amlodipine besylate [AML] by N-Bromosuccinimide [NBS] was investigated aqueous acidic medium under pseudo-first-order condition. The experimental results indicated that the reaction exhibits first-order concerning N-bromosuccinimide, fractional-order concerning [AML] and sulphuric acid [H2SO4]. There was no substantial effect on the rate of the reaction with KNO3. The reaction stoichiometry shows one mole of amlodipine besylate consumes one mole of n-bromosuccinimide. The effect of temperature on the reaction rate was studied, and the activation paramet

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12

Woo, Won, Sam Kang, and Sang-sup Jew. "Cycloetherification of Hydroxyoleanenes byN-Bromosuccinimide." Planta Medica 51, no. 06 (1985): 501–4. http://dx.doi.org/10.1055/s-2007-969575.

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13

Albertsson, J., and C. Svensson. "Solid-stateN-bromosuccinimide–bromide complexes." Acta Crystallographica Section A Foundations of Crystallography 43, a1 (1987): C69. http://dx.doi.org/10.1107/s0108767387083648.

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14

Song, Xianheng, Shanshui Meng, Hong Zhang, Yi Jiang, Albert S. C. Chan, and Yong Zou. "Dibrominated addition and substitution of alkenes catalyzed by Mn₂(CO)₁₀." Chemical Communications 57, no. 98 (2021): 13385–88. http://dx.doi.org/10.1039/d1cc04534b.

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15

Xu, Zoufeng, Zhigang Wang, Shek-Man Yiu, and Guangyu Zhu. "Mono- and di-bromo platinum(iv) prodrugs via oxidative bromination: synthesis, characterization, and cytotoxicity." Dalton Transactions 44, no. 46 (2015): 19918–26. http://dx.doi.org/10.1039/c5dt03101j.

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16

Li, Jian-Ping, Ping Liu, and Yu-Lu Wang. "An Efficient and Convenient Method for the synthesis of Acyldiazenes from Acylhydrazines." Journal of Chemical Research 2003, no. 2 (2003): 109–10. http://dx.doi.org/10.3184/030823403103173138.

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17

Yang, Tonghao, Weixia Wang, Dian Wei, Tianqi Zhang, Bing Han та Wei Yu. "Synthesis of quinazolinones via radical cyclization of α-azidyl benzamides". Organic Chemistry Frontiers 4, № 3 (2017): 421–26. http://dx.doi.org/10.1039/c6qo00656f.

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18

Bell, Jacob P., Jacqueline E. Cloud, Jifang Cheng, et al. "N-Bromosuccinimide-based bromination and subsequent functionalization of hydrogen-terminated silicon quantum dots." RSC Adv. 4, no. 93 (2014): 51105–10. http://dx.doi.org/10.1039/c4ra08477b.

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19

Naskar, Shibu, Susital Mal, Shivangi Shivangi, and Subrata Das. "A rapid and scalable method for visible light induced bromination of uracil derivatives in a falling film looping photoreactor." RSC Advances 14, no. 47 (2024): 34925–37. http://dx.doi.org/10.1039/d4ra05774k.

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20

Jung, Younjae, Taeil Shin, Kiseong Kim, et al. "Rh(0)/Rh(iii) core–shell nanoparticles as heterogeneous catalysts for cyclic carbonate synthesis." Chemical Communications 53, no. 2 (2017): 384–87. http://dx.doi.org/10.1039/c6cc08318h.

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21

Choi, Ji Yong, Chan Kyu Lim, Bumjin Park, Minjun Kim, Aqil Jamal, and Hyunjoon Song. "Surface activation of cobalt oxide nanoparticles for photocatalytic carbon dioxide reduction to methane." Journal of Materials Chemistry A 7, no. 25 (2019): 15068–72. http://dx.doi.org/10.1039/c9ta04323c.

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22

Lee, Yu Jeong, Myung Gil Choi, Tae Jung Park, and Suk-Kyu Chang. "Reaction-based fluorometric analysis ofN-bromosuccinimide by oxidative deprotection of dithiane." Analyst 144, no. 10 (2019): 3267–73. http://dx.doi.org/10.1039/c8an02125b.

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23

D’Aleo, Danielle N., Sheena R. Allard, Cassandra C. Foglia, et al. "Green halogenation of aromatic heterocycles using ammonium halide and hydrogen peroxide in acetic acid solvent." Canadian Journal of Chemistry 91, no. 8 (2013): 679–83. http://dx.doi.org/10.1139/cjc-2013-0058.

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The green generation of X+ (X = Br, I) using hydrogen peroxide in aqueous acetic acid allows access to aromatic heterocyclic halides in yields and purities comparable to syntheses employing N-bromosuccinimide. In activated and unsubstituted thiophene rings, regioselectivity is quantitative for positions α to the sulfur; pyrroles also give quantitative reactions, at least initially. Deactivated rings, including furans and thiazoles, as well as thiophenes with strongly electron-withdrawing groups showed little to no reactivity under the conditions investigated. The reaction shows remarkable func

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24

Gucchait, Arin, Kuladip Jana, and Anup Kumar Misra. "Convenient preparation of thioglycomimetics: S-glycosyl sulfenamides, sulfinamides and sulphonamides." RSC Advances 7, no. 52 (2017): 32478–87. http://dx.doi.org/10.1039/c7ra05339h.

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S-Glycosyl sulfenamide derivatives were rapidly prepared from glycosyl thiols using N-bromosuccinimide or N-chlorosuccinimide. Sulfenamide derivatives were oxidized to corresponding sulfinamides and sulfonamides.

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25

Shinde, Mahesh H., та Umesh A. Kshirsagar. "N-Bromosuccinimide promoted and base switchable one pot synthesis of α-imido and α-amino ketones from styrenes". Organic & Biomolecular Chemistry 14, № 3 (2016): 858–61. http://dx.doi.org/10.1039/c5ob02034d.

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26

Wu, Ya, Mengsha Zhang, Yanli Zhang, et al. "NBS-activated cross-dehydrogenative esterification of carboxylic acids with DMSO." Organic Chemistry Frontiers 7, no. 18 (2020): 2719–24. http://dx.doi.org/10.1039/d0qo00617c.

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27

Karunakaran, C., and C. Venkatachalapathy. "Methoxybromination of Cinnamic Acid byN-Bromosuccinimide." Bulletin of the Chemical Society of Japan 63, no. 8 (1990): 2404–7. http://dx.doi.org/10.1246/bcsj.63.2404.

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28

Svensson, C., J. Albertsson, and L. Eberson. "Caesium tris(N-bromosuccinimide)bromate(1-)." Acta Crystallographica Section C Crystal Structure Communications 42, no. 11 (1986): 1500–1502. http://dx.doi.org/10.1107/s0108270186091692.

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29

Haque, Inam U., Wajiha Akram, Shahid Iqbal, and Shamaila Sadaf. "Linear Sweep Voltammetry of N-Bromosuccinimide." ECS Transactions 13, no. 24 (2019): 71–76. http://dx.doi.org/10.1149/1.3013291.

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30

Shimizu, Sumio, Yoshiaki Imamura, and Tatsuo Ueki. "Incompatibilities between N-Bromosuccinimide and Solvents." Organic Process Research & Development 18, no. 2 (2014): 354–58. http://dx.doi.org/10.1021/op400360k.

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31

Zong, Zhi-Min, Wei-Hong Zhang, Qun Jiang, Jin Lu, and Xian-Yong Wei. "Photochemical Reactions of Hydroarenes withN-Bromosuccinimide." Bulletin of the Chemical Society of Japan 75, no. 4 (2002): 769–71. http://dx.doi.org/10.1246/bcsj.75.769.

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32

Xu, Hui, Rong-Lu Huang, Zhu Shu, Ran Hong, and Ze Zhang. "Chemoselective synthesis of 5,4′-imidazolinyl spirobarbiturates via NBS-promoted cyclization of unsaturated barbiturates and amidines." Organic & Biomolecular Chemistry 19, no. 22 (2021): 4978–85. http://dx.doi.org/10.1039/d1ob00508a.

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The cyclization of unsaturated barbiturates and amidines promoted by N-bromosuccinimide furnished a variety of structurally novel 5,4′-imidazolinyl spirobarbiturates with high chemoselectivity, good yields and remarkable functional group tolerance.

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33

Kulciţki, Veaceslav, Marina Cara, Andrea Bourdelais, Tomas Schuster, and Daniel Baden. "Synthesys of a Functionalized Tetrahydrofuran Fragment Through Bromination-Cyclization of a Conjugated Diene." Chemistry Journal of Moldova 5, no. 1 (2010): 118–20. http://dx.doi.org/10.19261/cjm.2010.05(1).13.

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Conjugate 1,4-addition of N-bromosuccinimide (NBS) to a diene system, possessing a suitable oxygen functionality, leads to functionalized tetrahydrofuran derivatives, which can be further derivatized into different synthetic targets.

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34

Wang, Zhengmeng, Lili Lin, Pengfei Zhou, Xiaohua Liu, and Xiaoming Feng. "Chiral N,N′-dioxide-Sc(NTf2)3 complex-catalyzed asymmetric bromoamination of chalones with N-bromosuccinimide as both bromine and amide source." Chemical Communications 53, no. 24 (2017): 3462–65. http://dx.doi.org/10.1039/c7cc00470b.

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35

Bhardwaj, Nivedita, Ajit Kumar Singh, Nancy Tripathi, Bharat Goel, Arindam Indra, and Shreyans K. Jain. "Ni–NiO heterojunctions: a versatile nanocatalyst for regioselective halogenation and oxidative esterification of aromatics." New Journal of Chemistry 45, no. 31 (2021): 14177–83. http://dx.doi.org/10.1039/d1nj02777h.

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Herein, we report a facile method for the synthesis of Ni–NiO heterojunction nanoparticles, which we utilized for the nuclear halogenation reaction of phenol and substituted phenols using N-bromosuccinimide (NBS).

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36

Gong, Liang, Li-Juan Xing, Tong Xu, et al. "Metal-free oxidative olefination of primary amines with benzylic C–H bonds through direct deamination and C–H bond activation." Org. Biomol. Chem. 12, no. 34 (2014): 6557–60. http://dx.doi.org/10.1039/c4ob01025f.

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An oxidative olefination reaction between aliphatic primary amines and benzylic sp<sup>3</sup> C–H bonds has been achieved using N-bromosuccinimide as catalyst and tert-butyl hydroperoxide as oxidant.

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37

Saeed, Hani Yeslam, Devendra S. Wagare, Mujahed Shaikh, and Ayesha Durrani. "Microwave-promoted One-pot Synthesis of Imidazo[1,2-a]pyridines in Lemon Juice." Current Microwave Chemistry 7, no. 3 (2020): 238–43. http://dx.doi.org/10.2174/2213335607999201008144429.

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Objective: A simple and highly efficient microwave-promoted procedure for the synthesis of imidazo[1,2-a]pyridine derivatives from the reaction of aromatic ketones, N-bromosuccinimide, and 2-aminopyridines in lemon juice was designed. The main advantages of this protocol, such as clean reaction profile, mild reaction condition, high yield, and minimum reaction time, were compared to other previously developed methods. Method: A mixture of aromatic ketones (1a-m) (0.005 m), N-bromosuccinimide (NBS) (0.005 m), and lemon juice (10 ml) was irradiated by microwave at 400-watt power at 85°C, and the

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38

Kraus, George A., and Shuai Wang. "The Dianion of Dehydroacetic Acid: A Direct Synthesis of Pogopyrone A." Synthesis 52, no. 10 (2020): 1541–43. http://dx.doi.org/10.1055/s-0037-1610752.

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Dehydroacetic acid was converted into a silyl enol ether and titanium enolate. These reacted effectively with aldehydes and N-bromosuccinimide. Oxidation of the adduct with benzaldehyde afforded pogopyrone A in excellent overall yield.

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39

Desvard, Osvaldo E., Maria F. Rozas, and Maria V. Mirífico. "Light-catalyzed bromination of 3,4-dimethyl-1,2,5-thiadiazole with N-bromosuccinimide." Collection of Czechoslovak Chemical Communications 54, no. 8 (1989): 2176–80. http://dx.doi.org/10.1135/cccc19892176.

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1H NMR study of light-catalyzed bromination of 3,4-dimethyl-1,2,5-thiadiazole with N-bromosuccinimide has been carried out in order to reach conclusions on synthetic possibilities and relative reactivities of several products formed.

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40

Mondal, Haripriyo, Md Raja Sk, and Modhu Sudan Maji. "Cooperativity within the catalyst: alkoxyamide as a catalyst for bromocyclization and bromination of (hetero)aromatics." Chemical Communications 56, no. 77 (2020): 11501–4. http://dx.doi.org/10.1039/d0cc04673f.

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Alkoxyamide has been reported as a catalyst for the activation of N-bromosuccinimide to perform bromocyclization and bromination of a wide range of substrates in a lipophilic solvent with adequate suppression of the background reactions.

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41

Sh. Alenezi, Samya, Ayman A. Gouda, Ragaa El Sheikh, et al. "Evaluation of the greenness profiles of indirect spectrophotometric methods for estimation of gemifloxacin mesylate in pure and dosage forms utilizing N-bromosuccinimide as a green reagent." Bulletin of the Chemical Society of Ethiopia 39, no. 2 (2024): 227–42. http://dx.doi.org/10.4314/bcse.v39i2.4.

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A validated, sensitive, user-friendly, precise, and dependable spectrophotometric technique has been developed to accurately detect the concentration of gemifloxacin mesylate in pure and dosage forms. The methods utilize N-bromosuccinimide as an eco-friendly oxidizing agent in acidic circumstances. The residual N-bromosuccinimide is measured by subjecting it to a chemical reaction with preset amounts of dyes, amaranth, methylene blue, and indigocarmine and the absorbance is measured at λmax of 520, 664 and 610 nm, respectively. The analytical technique was implemented and validated by thorough

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42

Jastrzebska, Izabella. "Preparation ofα-Bromoketones Involving the Reaction of Enol Triethyl Borates with N-Bromosuccinimide". Journal of Chemistry 2013 (2013): 1–4. http://dx.doi.org/10.1155/2013/294107.

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The ketones (5α- and 5β-cholestan-3-one and (1S,7aS)-1-tert-butoxy-hexahydro-7a-methyl-1H-inden-5-one) were efficientlyα-monobrominated by treatment of the corresponding enol triethyl borates with N-bromosuccinimide (NBS).

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43

Pan, Siqi, Xichuan Yang, Bin Cai, et al. "N-Bromosuccinimide as a p-type dopant for a Spiro-OMeTAD hole transport material to enhance the performance of perovskite solar cells." Sustainable Energy & Fuels 5, no. 8 (2021): 2294–300. http://dx.doi.org/10.1039/d1se00043h.

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Low cost N-bromosuccinimide (NBS) was applied as an effective p-type dopant in 2,2′,7,7′-tetrakis[N,N-di(4-methoxyphenyl)amino]-9,9-spirobifluorene (Spiro-OMeTAD), an important hole transport material (HTM) for perovskite solar cells (PSCs).

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44

Luo, Han, Zongyuan Tang, Tao Wang, et al. "Regioselective N1- and N2-heterocycloalkylation of N1-sulfonyl-1,2,3-triazoles." Organic Chemistry Frontiers 7, no. 22 (2020): 3727–33. http://dx.doi.org/10.1039/d0qo01111h.

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A tuneable and visible-light-driven three-component reaction between N<sup>1</sup>-sulfonyl-1,2,3-triazoles, saturated heterocycles, and N-bromosuccinimide for regioselective synthesis of N<sup>1</sup>- or N<sup>2</sup>-heterocycloalkylated 1,2,3-triazoles.

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45

Bar, Sukanta. "Organocatalysis in the stereoselective bromohydrin reaction of alkenes." Canadian Journal of Chemistry 88, no. 7 (2010): 605–12. http://dx.doi.org/10.1139/v10-053.

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An efficient regio- and stereo-selective (>99:1) trans-bromohydrination (bromohydroxylation and bromomethoxylation) of alkenes including α,β-unsaturated carbonyl compounds with N-bromosuccinimide (NBS) has been achieved by using 1.0 mol% of N,N′-diarylthiourea catalyst.

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46

Chatterjee, Nachiketa, Divya Bhatt, and Avijit Goswami. "A novel transition metal free [bis-(trifluoroacetoxy)iodo]benzene (PIFA) mediated oxidative ipso nitration of organoboronic acids." Organic & Biomolecular Chemistry 13, no. 17 (2015): 4828–32. http://dx.doi.org/10.1039/c5ob00337g.

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A mild, convenient and transition metal free methodology for oxidative ipso nitration of organoboronic acids, including heteroaryl- and alkylboronic acids, has been developed using a combination of [bis-(trifluoroacetoxy)]iodobenzene (PIFA) – N-bromosuccinimide (NBS) and sodium nitrite as the nitro source.

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47

Zysman-Colman, Eli, Karla Arias, and Jay S. Siegel. "Synthesis of arylbromides from arenes and N-bromosuccinimide (NBS) in acetonitrile — A convenient method for aromatic bromination." Canadian Journal of Chemistry 87, no. 2 (2009): 440–47. http://dx.doi.org/10.1139/v08-176.

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Abstract:

Regioselective and chemoselective electrophilic bromination of a wide series of activated arenes using N-bromosuccinimide (NBS) in acetonitrile occurs readily. Environmentally friendly conditions, large substrate scope, and ease of synthesis enhance the utility of this method over other electrophilic bromination conditions.

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48

Merkhatuly, N., S. K. Zhokizhanova, L. T. Balmagambetova, and S. M. Adekenov. "Stereoselective carbocyclization of hanphyllin with N-bromosuccinimide." Russian Journal of General Chemistry 76, no. 8 (2006): 1345–46. http://dx.doi.org/10.1134/s1070363206080378.

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49

Abdel-Wadood, Hanaa M., Niveen A. Mohamed, and Fardous A. Mohamed. "Spectrofluorimetric Determination of Acetaminophen with N-Bromosuccinimide." Journal of AOAC INTERNATIONAL 88, no. 6 (2005): 1626–30. http://dx.doi.org/10.1093/jaoac/88.6.1626.

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Abstract A simple, sensitive, and selective method for determination of acetaminophen based on its oxidation using N-bromosuccinimide (NBS) to produce a highly fluorescent product. Optimization of reaction variables was carried out concerning NBS concentration, pH, temperature, reaction time, and stability time. Under optimal analytical conditions, the fluorescent intensity was measured at λemission. 442 nm (excitation at λ 330 nm). The linearity range is 120–800 ng/mL with lower detection limit of 33.6 ng/mL acetaminophen. The method was applied successfully to the determination of the compou

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50

Chang, Meng-Yang, and Chieh-Kai Chan. "N-Bromosuccinimide-Mediated Synthesis of Substituted Quinoxalines." Synthesis 48, no. 21 (2016): 3785–93. http://dx.doi.org/10.1055/s-0035-1561472.

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