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Dissertations / Theses on the topic 'Ethynyl ketone'

Author: Grafiati

Published: 10 December 2022

Last updated: 31 July 2025

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1

Kitagawa, Kristen. "Studies in the asymmetric reduction of (3s)-3-amino-1-chloro-4-phenyl-2-butanone derivatives." Diss., Georgia Institute of Technology, 2010. http://hdl.handle.net/1853/39464.

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This thesis focuses on the asymmetric reduction of N-protected derivatives of (3S)-3-amino-1-chloro-4-phenyl-2-butanone to their corresponding diastereomeric alcohol products, which are key intermediates in the synthesis of HIV protease inhibitors. Although the stereoselective synthesis of the (S,S) alcohol product is easily achieved, preparing the (R,S) diastereomer is much more challenging. I investigated three diastereoselective reduction processes: 1) Meerwein-Ponndorf-Verley (MPV) reduction, 2) asymmetric transfer hydrogenation, and 3) boron reducing agents. The diastereoselectivity of

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2

Abu-Khumra, Sabah. "Quantum rotor tunnelling in methyl ethyl ketone and acetophenone studied using field-cycling NMR techniques." Thesis, University of Nottingham, 2013. http://eprints.nottingham.ac.uk/14032/.

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In the solid state the rotation of a methyl group is hindered by a potential barrier and at low temperature the rotational motion is characterised by quantum tunnelling. The Pauli Exclusion Principle imposes constraints on the allowable eigenstates of the methyl rotor and leads to a combination of spatial and spin variables. The characteristics of these quantum tunnelling states, labelled A and E, are explored experimentally and methods are investigated for creating prescribed non-equilibrium states. We will investigate and explore the tunnelling polarization associated with the A and E tunnel

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3

Van, Bergen Barry. "Diacetyl : identification and characterisation of molecular mechanisms for reduction in yeast and their application in a novel enzyme based assay for quantification in fermentation systems." Thesis, McGill University, 2006. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=103015.

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Diacetyl (2,3-butanedione) is an important flavour active, oxidative compound that has significant impact on cellular health as well as financial impact in industrial fermentations. The presence of diacetyl in certain fermented beverages, such as beer, results in an unpleasant butterscotch-like flavour and its concentration needs to be reduced by yeast to below the taste threshold prior to filtration and packaging. This results in significant process inefficiency. Furthermore, diacetyl negatively impacts cellular health and has been associated with neurodegenerative diseases and general cell a

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4

Bouex-Godeau, Isabelle. "Myocardite toxique aprés ingestion de Butanox : à propos d'une observation." Bordeaux 2, 1992. http://www.theses.fr/1992BOR2M099.

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5

Guzman, Barrera Nydia Ileana. "Eco-compatible syntheses of bio-based solvents for the paint and coating industry." Thesis, Toulouse, INPT, 2018. http://www.theses.fr/2018INPT0050/document.

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La production mondiale de solvants représente environ 28 millions de tonnes, dont 5 millions en Europe. L’industrie des peintures et des revêtements en est la principale consommatrice (46 % des solvants produits). Dans ce domaine, les solvants les plus utilisés sont l'acétate d'éthyle, l'acétate de butyle et la méthyl éthyl cétone. Ces molécules sont actuellement synthétisées industriellement à partir de substrats d’origine pétrochimique en présence de catalyseurs homogènes et dans des conditions énergivores. Afin de réduire l’impact environnemental des peintures et revêtements, la substitutio

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6

Kotdawala, Rasesh R. "Adsorption studies of hazardous air pollutants in microporous adsorbents using statistical mechanical and molecular simulation techniques." Worcester, Mass. : Worcester Polytechnic Institute, 2007. http://www.wpi.edu/Pubs/ETD/Available/etd-050407-112429/.

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Dissertation (Ph.D.) -- Worcester Polytechnic Institute.<br>Keywords: Activated carbons; Hydrogen cyanide; Methyl ethyl ketone; Adsorption; Mercury; Monte-Carlo; Solvents; Molecular simulations; Zeolites; Water; Methanol; Nanopores. Includes bibliographical references (leaves 147-150).

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7

Pham, Van Toan, Thi Phuong Nguyen, and Thanh Giao Nguyen. "Indoor air quality and health risk assessment for workers in packaging production factory, Can Tho city, Viet Nam." Technische Universität Dresden, 2018. https://tud.qucosa.de/id/qucosa%3A33338.

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The production of packaging goods for cement is one of the most important industries, contributing to income of many workers. Production activities, however, cause air pollution and health risk. The study was conducted to assess air quality and health risks of workers through air quality data and interviewing employees from 2016-2017 at a packaging production factory, Can Tho city, Vietnam. The findings indicated that temperature and noise exceeded the national technical regulations (QCVN 22-26: 2016/TT-BYT) while the humidity, wind speed, light, respirable particles, toxic gases (benzene, tol

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8

Huchede, Maxime. "Développement de procédés originaux et compétitifs de synthèse de méthionine, à partir de nouvelles matières premières." Thesis, Lyon, 2017. http://www.theses.fr/2017LYSE1288.

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9

Renaud, Jean-Paul. "Oxydations d'alcanes et d'alcènes par des systèmes métalloporphyriniques modelés du cytochrome P-450." Paris 6, 1986. http://www.theses.fr/1986PA066139.

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La synthèse d'une pophyrine de fer à "anses de panier" chirale comportant des aminoacidés de configuration déterminée est décrite. On a étudié sa pureté optique et sa conformation en solution. Dans une deuxième partie on décrit un nouveau système oxydant catalytique utilisant l'eau oxygénée en présence d'une porphyrine de manganèse et d'imidazole permettant la conversion quantitative d'alcènes en époxydes et d'alcanes en alcools et cétones.

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10

Parker, Christian Richard. "Polarised alkynyl ruthenium complexes." Thesis, 2010. http://hdl.handle.net/2440/65307.

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Chapter 1 outlines the potential application of metal alkynyl complexes and then describes the different methods in the literature for the synthesis of alkynyl, poly-ynyl and homo- and hetero-metal complexes. Their chemistry will then be discussed. This Chapter concludes with an outline of the work to be described in the remainder of the thesis. Chapter 2 describes a series of complexes containing a new tricyanovinylethynyl (3,4,4-tricyanobut-3-en-1-ynyl) ligand obtained by direct substitution of a CN group in tetracyanoethene by ethynyl complexes M(C=CH)(PP)Cp' [M = Ru, Os, (PP)Cp' = (PPh₃)₂C

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11

Yeh, Po-Yin, and 葉博寅. "Thermal Hazard Analysis of Methyl Ethyl Ketone Peroxide." Thesis, 2001. http://ndltd.ncl.edu.tw/handle/69812189499623175414.

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碩士<br>國立雲林科技大學<br>環境與安全工程系碩士班<br>89<br>In the past forty years in Japan and Taiwan, many thermal explosions have been caused by methyl ethyl ketone peroxide (MEKPO) under the influence of external fire. Thermograms of commercialized MEKPO with dimer were first screened by Differential Scanning Calorimetry (DSC) to determine the heat of decomposition and exothermic onset temperature. Thermal runaway phenomena were then thoroughly investigated by Vent Sizing Package2. (VSP2) Data of thermokinetics and thermal analysis were used for hazard evaluation of MEKPO thermal explosions. Instea

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12

Jong, Jen-Yu, and 鍾鎮宇. "Binary Adsorption Isotherms of Methyl Ethyl Ketone/ Methyl Isobutyl Ketone Aqueous Solution on Activated Carbon." Thesis, 2006. http://ndltd.ncl.edu.tw/handle/28923354136053080651.

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碩士<br>長庚大學<br>化工與材料工程研究所<br>94<br>The objective of this research is to obtain the adsorption equilibrium data of the liquid binary-component solution of MEK and MIBK at room temperature on the granular activated carbon in an agitated adsorption vessel. The goal is to examine the adsorption isotherm of the binary-component system with the single-component adsorption isotherm. Langmuir isotherm can well express both the single component adsorption isotherm of MEK and MIBK on activated carbon. The concentration of MEK and MIBK in the fluid phase discussed in the adsorption in the adsorption isot

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13

Fong-Cheng, Kao, and 高逢成. "Catalytic Incineration of Methyl Ethyl ketone over Ferrite Catalysts." Thesis, 2011. http://ndltd.ncl.edu.tw/handle/60088246117854510991.

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碩士<br>國立高雄應用科技大學<br>化學工程與材料工程系<br>99<br>Methyl Ethyl Ketone (MEK) is a popular solvent/lotion in semiconductor industry, PU leather industry, tape manufacturing industry, and electronic industry. Due to the exhaust of manufacturing process, MEK becomes one of the main sources of the volatile organic compounds. Its harmful to human and surrounding environment cannot be regardless because of its large amount. This study investigates the incineration feasibility of MEK on seven kinds of ferrites (Cu-ferrite, Mn-ferrite, Zn-ferrite, Co-ferrite, Ni-ferrite, Cr-ferrite, Pure-ferrite) synthesized by

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14

chang, chin-kuei, and 張晉魁. "Treatment of Methyl Ethyl Ketone vapor by the photocatalytic process." Thesis, 2006. http://ndltd.ncl.edu.tw/handle/02271271831832719899.

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碩士<br>長庚大學<br>化工與材料工程研究所<br>94<br>This research discuss mainly UV/TiO2 process in the continuous packed bed reactor. We use glass pearls for loading TiO2.The gaseous phase pollutant is Methyl Ethyl Ketone (MEK) .The changes of this experiment includes such effects as wavelength of UV light , initial concentration, system temperature, flow rate and retention time, etc. Then we combine Langmuir-Hinshelwood adsorption theory with Fick mass transfer theory for examining the kinetic equation suitable for this experimental system. Find out several parameter such as L-H reaction rate constant (k) , M

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15

Tseng, Jo-Ming, and 曾若鳴. "Thermal Hazard and Incompatible Reaction Mechanism for Methyl Ethyl Ketone Peroxide." Thesis, 2008. http://ndltd.ncl.edu.tw/handle/63595752629604042490.

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博士<br>雲林科技大學<br>工程科技研究所博士班<br>96<br>The thermal stability of solutions of methyl ethyl ketone peroxide (MEKPO) dissolved in dimethyl phthalate (DMP), with the presence of inorganic acids (HCl, HNO3, H3PO4, and H2SO4) and the other incompatible materials as contaminants had been studied. MEKPO is extensively employed in the chemical industries. Several severe fires and explosions have been induced by MEKPO in East Asia during the last four decades. Therefore, this study was conducted with a view to realize its essentially hazardous characteristics. In this study, we used differential scanning

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16

Tseng, Jo-Ming, and 曾若鳴. "Incompatible Hazard Analysis on Methyl Ethyl Ketone Peroxide with Inorganic Acid." Thesis, 2005. http://ndltd.ncl.edu.tw/handle/37985244477001310959.

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碩士<br>國立雲林科技大學<br>環境與安全工程系碩士班<br>93<br>Historically, methyl ethyl ketone peroxide (MEKPO), a universal hardener in the rubber industries, has caused many serious explosions and fires in Taiwan, Japan, Korea, and China. This study used certain thermal analytical methods to thoroughly explore both why MEKPO led to these accidents and what happened during the upset conditions. Potential process contaminants (inorganic acids), such as HNO3、H3PO4、HCl、H2SO4, were deliberately selected to mix with MEKPO for discussing the exothermic phenomenon. Differential scanning calorimetry (DSC) and Vent Sizing

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17

Chang, Ron-Hsin, and 張榮興. "Thermal Runaway Hazard Analysis on Methyl Ethyl Ketone Peroxide with Incompatible Substances." Thesis, 2003. http://ndltd.ncl.edu.tw/handle/95211091788503455375.

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碩士<br>國立雲林科技大學<br>環境與安全工程系碩士班<br>91<br>In the past four decades in Japan, Taiwan and China, Methyl Ethyl Ketone Peroxide (MEKPO) has caused many thermal explosions hazard with its thermal instability and incompatibility. In this study, the thermal decomposition and runaway behaviors of MEKPO with about 1 wt % incompatibilities such as H2SO4, HCl, NaOH, KOH, Fe2O3, FeCl3, and FeSO4 were analyzed by DSC (Differential Scanning Calorimetry) thermal analysis and VSP2 (Vent Sizing Package2) adiabatic calorimetry. The thermokinetic data, such as onset temperature, heat of decomposition, adiabatic tem

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18

Al-Auda, Zahraa Fadhil Zuhwar. "Conversion of methyl ethyl ketone (MEK) to valuable chemicals over multifunctional supported catalysts." Diss., 2018. http://hdl.handle.net/2097/39274.

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Doctor of Philosophy<br>Department of Chemical Engineering<br>Keith L. Hohn<br>The present work describes the conversion of bio-derived methyl ethyl ketone (MEK) into different useful chemicals. The first part discusses the direct conversion of MEK to butene over supported copper catalysts (Cu-Al₂O₃, Cu-zeolite Y sodium (Cu-ZYNa) and Cu-zeolite Y hydrogen (Cu-ZYH)) in a fixed bed reactor. In this reaction, MEK is hydrogenated to 2-butanol over metal sites, and further dehydrated on acid sites to produce butene. Experimental results showed that the selectivity of butene was the highest over Cu

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19

Chang, Ron-Hsin, and 張榮興. "Thermal Runaway Hazard and Incompatible Reaction Analysis for Organic Peroxide - Methyl Ethyl Ketone Peroxide." Thesis, 2007. http://ndltd.ncl.edu.tw/handle/96938517439457791329.

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博士<br>國立中興大學<br>化學工程學系所<br>96<br>Methyl ethyl ketone peroxide (MEKPO) is extensively employed in the chemical industries. In the past four decades, several thermal explosions hazard with its thermal instability and incompatibility caused fires and explosions have been induced by MEKPO in East Asia. In this study, the thermal decomposition and runaway behaviors of MEKPO with about 1 mass % incompatibilities such as H2SO4, HCl, NaOH, KOH, Fe2O3, FeCl3, and FeSO4 were analyzed by differential scanning calorimetry (DSC) with the following kinetics evaluation to identify the root-cause of the runaw

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20

Cheng, Fu-Hsien, and 鄭富賢. "Applied ALOHA simulation toluene, methyl ethyl ketone, cyclohexanone consequence analysis of hazards tank leak." Thesis, 2015. http://ndltd.ncl.edu.tw/handle/03394896210084583870.

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碩士<br>國立雲林科技大學<br>環境與安全衛生工程系<br>103<br>Abstract The study is based on a chemical plant in Kaohsiung Linyuan Industrial Area. We used ALOHA (Area Location of Hazardous Atmosphere) analysis and simulation software, according to the geographical location and environmental characteristics. To predict the harmful gas diffusion distribution, after the toluene, methyl ethyl ketone, cyclohexanone, etc.tanks leakage caused by the earthquake. The diffusion results (Figure footprint footprint) nested a Google Earth map, discussed the following items, as a reference to take appropriate control measures a

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21

Xie, Zhao-Cheng, and 謝照晟. "Study on Chemical Looping Combustion Procedure of Organic Waste Solvent-Methyl Ethyl Ketone Treatment." Thesis, 2019. http://ndltd.ncl.edu.tw/handle/3mb8dp.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>107<br>The tech industry becomes the major industry in Taiwan gradually due to the increase in the demand of computer, communication, and consumer electronics. The amount of organic solvent used for manufacture thus is increased sharply. Some companies assign waste treatment companies to incinerate these waste solvent, resulting in plenty of air pollution and energy consumption. The chemical looping combustion (CLC) is a novel combustion process with flameless, high combustion efficiency, and direct separation of carbon dioxide. The operation conditions, such as reac

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22

Qiu-Wei, Shun-Xin, and 邱魏順鑫. "Hearing Loss in Aircraft Maintenance Works Exposed to Noise, n-Hexane, and Methyl Ethyl Ketone." Thesis, 2009. http://ndltd.ncl.edu.tw/handle/70051461984182258462.

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碩士<br>中國醫藥大學<br>環境醫學研究所碩士班<br>97<br>Noise has been documented as the most important hazard about hearing loss, especially at occupational settings. Aircraft maintenance workers are at the high risk of hearing loss associated with a great amount of noise exposure at work such as regular check of airplane taking off and landing. Organic solvents exposure has been noted as an additional factor of hearing loss among aircraft maintenance workers. Previous studies have revealed that organic solvents related occupational hearing loss might be due to the ototoxicity after exposure in workers. N-hexane

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23

Lin, I.-Tso, and 林奕佐. "The Study of Reaction of Methyl Ethyl Ketone and 3-Methyl-2-Butanone with Ozone." Thesis, 2019. http://ndltd.ncl.edu.tw/handle/577xta.

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碩士<br>義守大學<br>化學工程學系暨生物技術與化學工程研究所<br>107<br>Butanone (MEK) and 3-methyl-2-butanone (MIPK) are volatile organic compounds (VOCs), and often used in factories as solvents, dewaxing agents and cleaning agents, which will lead to water and air pollution. Ozone can effectively decompose organic compounds due to its highly oxidizing properties. This research was applied the high oxidation capacity of ozone to study the products of reaction of ozone with methyl ethyl ketone and 3-methyl-2-butanone. The results will helpful for understanding the oxidation mechanism of oxidation reaction by ozone. T

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24

Liao, Zhi Min, and 廖致民. "Photocatalytic degradation of toluene, methyl ethyl ketone and methylene blue using B/V codoped titanium dioxide." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/17827579723597465611.

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25

Yun, Yuan-Der, and 雲遠德. "Biological monitoring of occupational exposure to the mixture of N,N-dimethylformamide, methyl ethyl ketone, and toluene." Thesis, 2004. http://ndltd.ncl.edu.tw/handle/15393908810360752176.

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碩士<br>國立成功大學<br>環境醫學研究所<br>92<br>The exposure of the humans to the chemical mixtures is the general rule in the general environment as well as in most occupational settings. Lower toxicity or higher toxicity from mixtures than the expected depends on their constituents and potencies. It is very likely that the workers could be exposed to N,N-dimethylformamide (DMF), methyl ethyl ketone (MEK), and toluene (TOL) in the occupational environments simultaneously. This study was aimed to investigate the effects of the different co-exposure levels of MEK and toluene and different DMF on different bio

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26

Hwang, Jiun Jye, and 黃俊傑. "Performance Study for Bioconversion of Methyl Ethyl Ketone (MEK) in Wasted Gas Streams by A Biotrickling Filter." Thesis, 1994. http://ndltd.ncl.edu.tw/handle/71346859917726281139.

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27

Wu, Hung-Ming, and 吳泓明. "ADSORPTION/OXIDATION OF METHYL-ETHYL-KETONE VAPOR WITH OZONE ON ACTIVATED CARBON AND ACTIVATED CARBON WITH MO-CVD." Thesis, 2006. http://ndltd.ncl.edu.tw/handle/15322082432822534765.

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博士<br>長庚大學<br>化工與材料工程研究所<br>95<br>This study attempts to combine the technologies of adsorption of volatile organic compound (VOC) on activated carbon and oxidation of VOC by O3. In the adsorption/oxidation process, the effects of ozone for the adsorption characteristics of methyl ethyl ketone (MEK) vapor on activated carbon are investigated. The kinetic parameters of reaction for MEK vapor and O3 on activated carbon are also determined. The results show that the destructive efficiencies of MEK by 1000 ppmv O3 on activated carbon are from 12.4 % to 48.5 %. From the power law kinetic model, t

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28

Tseng, Chih-Hao, and 曾志豪. "Effects of co-exposure to occupational noise and methyl ethyl ketone on 24-hour ambulatory blood pressure in aviation industry workers." Thesis, 2011. http://ndltd.ncl.edu.tw/handle/39730834721588276556.

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碩士<br>中國醫藥大學<br>職業安全與衛生學系碩士班<br>99<br>Objectives: The repeated-measure study was to investigate effects of co-exposure to occupational noise and methyl ethyl ketone (MEK) on ambulatory blood pressure among aviation industry workers. Methods: We selected an aircraft manufacturing company to recruit 145 volunteers as the study population. These workers were classified into five different-exposure groups based on their individual noise levels and MEK concentrations at work, including the co-exposure (≥71.2 dBA; MEK ≥1.182 ppm), noise-exposure (≥71.2 dBA; MEK <1.182 ppm), MEK-exposure (<71.2 dBA;

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29

Shie, Jiun-Jie, and 謝俊結. "Samarium Diodide Promoted Reductive Coupling Reactions of Ethyl 2-Thiophenecarboxylate with Ketones. Applications to the Synthesis of Liquid Crystals and Photochromism." Thesis, 2002. http://ndltd.ncl.edu.tw/handle/27199427311265120771.

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碩士<br>國立臺灣大學<br>化學研究所<br>90<br>Abstract In this thesie, I describe the reductive double electrophilic coupling reactions of ethyl thiophene-2-carboxylate and ketones promoted by SmI2/HMPA and application of these compounds in the areas of liquid crystals and photochromism are under study. Ethyl thiophene-2-carboxylate underwent the reductive double electrophilic coupling reactions with aryl ketones by promotion of SmI2/HMPA to give disubstituted 4,5-dihydrothiophene-2-carboxylates in high regio- and stereoselective manner. The products obtained from the reductive

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30

Venkateswaran, Lakshmi 1965. "Effect of n-3 vs n-6 fatty acids and methyl ethyl ketone peroxide on adipose tissue cellularity, muscle weight, and lipoprotein lipase activity in rats." Thesis, 1993. http://hdl.handle.net/1957/26056.

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Carlsson, Henrik. "Development of an adductomic approach to identify electrophiles in vivo through their hemoglobin adducts." Doctoral thesis, 2016. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-129248.

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Humans are exposed to electrophilically reactive compounds, both formed endogenously and from exogenous exposure. Such compounds could react and form stable reaction products, adducts, at nucleophilic sites in proteins and DNA. The formation of adducts constitutes a risk for effects, such as cancer and contact allergy, and plays a role in ageing processes. Adducts to proteins offer a possibility to measure electrophilic compounds in vivo. Adductomic approaches aim to study the totality of adducts, to specific biomolecules, by mass spectrometric screening. This thesis describes the development

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