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Dissertations / Theses on the topic 'Imine chemistry'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Hammond, Max Leonard. "Imine catalyst stability." Thesis, University of Warwick, 2006. http://wrap.warwick.ac.uk/1172/.

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Chapter 1 presents a review of the background and current research regarding Schiff-base olefin polymerization catalysts, with special reference to the salicylaldimine species. An attempt is made to review trends within the current literature. Chapter 2 describes the synthesis and polymerization properties of tetradentate ligands with a bibenzyl backbone at titanium and zirconium centres, prepared with the intent of sterically hindering a 1,2-Migratory Insertion into the ligand imine functionality. A custom-built polymerization reactor was used to determine the stability of the catalytic syste

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2

Childs, Laura Jennifer. "Supramolecular assemblies based on imine and azo chemistry." Thesis, University of Warwick, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.269076.

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3

McMeekin, Peter. "Mechanistic aspects of imine cycloadditions." Thesis, Queen's University Belfast, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.356894.

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4

Rajviroongit, Shuleewan. "Cyclisation and cycloaddition of imine derivatives." Thesis, Queen's University Belfast, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.335436.

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5

Bhat, Shreesha V. "Synthesis of 1,2,4 oxadiazol-5-imine, 1,2,4-triazol-3-imine and derivatives : a substituted cyanamide-based strategy for heterocycle synthesis." Thesis, University of Lincoln, 2017. http://eprints.lincoln.ac.uk/28632/.

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Considering the importance of nitrogen-rich heterocycles in drug discovery, a novel strategy towards heterocycle synthesis was envisioned using cyanamide chemistry. Synthesis which involve mild conditions, avoids multi-step sequence and non-toxic reagents are desirable for generation of large combinatorial libraries of drug molecules. We envisaged that the NCN linkage of the cyanamide as well as the concomitant use of the nucleo-and electrophilic centres of the cyanamide could provide a novel synthetic route towards nitrogen heterocycles. The first part (Ch-2) constitute the bulk of the thesis

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6

Neshat, Abdollah. "Group V Imido Complexes Bearing Mono-Anionic Acetophenone Imine Ligands." University of Toledo / OhioLINK, 2011. http://rave.ohiolink.edu/etdc/view?acc_num=toledo1302269375.

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7

Beirl, Toni Marie. "Synthesis and Characterization of Novel Imine-Linked Covalent Organic Frameworks." The Ohio State University, 2015. http://rave.ohiolink.edu/etdc/view?acc_num=osu1437559176.

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8

Prema, Dipesh. "Different coordination modes of bis(imine-ridine) and bis(quinaldine) ligands." Diss., Manhattan, Kan. : Kansas State University, 2007. http://hdl.handle.net/2097/267.

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9

Hanton, Martin John. "Coordination complexes of bidentate phosphino-imine ligands : synthesis, characterisation and reactivity." Thesis, University of Leicester, 2003. http://hdl.handle.net/2381/33724.

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This thesis describes the synthesis, reactivity and coordination chemistry of a range of bidentate phosphino-imine ligands. The reactivity of the resultant complexes is also probed, while testing of the complexes for catalytic activity in a range of carbon-carbon bond-forming reactions is documented. Chapter 1 introduces the concepts of 'hemi-lability' and 'trans-influence', along with heteroditopic bidentate ligands, and specifically examines imine- and phosphine-based ligands, particularly aminophosphines. The nature of the phosphorus centre in terms of its steric and electronic properties i

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10

Stafford, Carolyne. "The sequential insertion of carbon monoxide and imines into nickel-carbon sigma-bonds and kinetic analysis of imine insertion into palladium-acyl sigma-bonds." Thesis, McGill University, 2007. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=18447.

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ABSTRACT The Sequential Insertion of Carbon Monoxide and Imines into Nickel-Carbon Sigma-Bonds and Kinetic Analysis of Imine Insertion into Palladium-Acyl Sigma-Bonds The coupling of imines and carbon monoxide mediated by late transition metals has been previously reported in the Arndtsen laboratory. The fundamental properties of 2,1-migratory insertion of imines into nickel- and palladium-acyl bonds are presented in this text. This study investigates the use of neutral eta2-N,O-salicylaldiminato nickel (II) systems (Chapter 2) as potential complexes to mediate the sequential insertion of

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11

Mugo, Jane Ngima. "Metal complexes based on monomeric and dendrimeric pyrrole-imine ligands as catalytic precursors." Thesis, University of the Western Cape, 2007. http://etd.uwc.ac.za/index.php?module=etd&action=viewtitle&id=gen8Srv25Nme4_7455_1242709415.

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<p>Over the recent past, organometallic chemistry has grown and the impact of catalytic applications in various chemical technologies has rapidly evolved from the realm of academic laboratories into full-scale industrial processes. Pyrrole-imine ligands were prepared by condensation of pyrrole-2-carboxylaldehyde with propyl amine, 2,6-diisopropylanaline, poly(propylene) imine dendrimer and 3-aminopropyl-triethoxysilane to give the desired ligands in good yields. These ligands were charaterized via combination of techniques to establish the molecular structure. Microanalysis was performed to co

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12

Deodhar, Bhushan S. "Towards the development of rotaxanes with two functional blocking groups." University of Cincinnati / OhioLINK, 2011. http://rave.ohiolink.edu/etdc/view?acc_num=ucin1311690891.

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13

De, Jongh Leigh-Anne. "Imine-donor complexes with group 6 and group 11 transition metals : coordination and dynamics." Thesis, Stellenbosch : Stellenbosch University, 2008. http://hdl.handle.net/10019.1/2001.

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Thesis (MSc (Chemistry and Polymer Science))--Stellenbosch University, 2008.<br>In this study the coordination of ligands with several coordination sites, 2-aminoazoles (2- amino-4-methylthiazole), 2-aminobenzothiazole, 2-aminobenzoimidazole and 2- aminothiazoline and a biguanidine (N-(2-methylphenyl)imidodicarbonimidic diamide) to soft metal centres [gold(I) (group 11), chromium(0) (group 6) and tungsten (0) (group 6)] was investigated. The aminoazoles have three coordination sites, an exocyclic amine nitrogen, an endocyclic imine nitrogen and an endocyclic thioether sulphur. The biguan

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14

GADDIRAJU, NARENDRA VARMA. "Asymmetric Synthesis of C-1 Substituted Cocaine Analogues Using Sulfinimine (N-Sulfinyl Imine) Chemistry And Vinylaluminum Addition to Sulfinimines (N-Sulfinyl Imines) For The Asymmetric Synthesis Of Alpha-Substituted-Beta-Amino Esters." Diss., Temple University Libraries, 2013. http://cdm16002.contentdm.oclc.org/cdm/ref/collection/p245801coll10/id/225834.

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Chemistry<br>Ph.D.<br>Organic nitrogen containing chiral compounds are widely found in nature, and a number of them exhibit important biological and medicinal properties. The main objective of this research is to develop new methods for the asymmetric synthesis of cocaine analogues having methyl (Me), ethyl (Et), n-propyl (n-Pr), n-pentyl (n-C5H11) and phenyl (Ph) groups at the C-1 bridgehead position. The second project concerned the asymmetric synthesis of anti-α-alkyl substituted beta-amino esters, a new chiral building block, utilizing chiral sulfinimine (N-sulfinyl imine) chemistry. The e

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15

Volbeda, Jeroen [Verfasser]. "The coordination chemistry of edge-bridged open indenyl and imidazolin-2-imine ligands / Jeroen Volbeda." München : Verlag Dr. Hut, 2014. http://d-nb.info/1058284908/34.

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16

Wiznycia, Alexander V. "The preparation and study of Bis(pyridyl-imine) and Monohelical salen-type complexes of iron and zinc." Diss., Manhattan, Kan. : Kansas State University, 2006. http://hdl.handle.net/2097/200.

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17

Kulchat, Sirinan. "Dynamic covalent chemistry of C=N, C=C and quaternary ammonium constituents." Thesis, Strasbourg, 2015. http://www.theses.fr/2015STRAF018/document.

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Cette thèse décrit la Chimie Covalente Dynamique (CCD) des échanges imine/imine, Knoevenagel/imine et Knoevenagel/Knoevenagel. La L-proline est un excellent organocatalyseur pour la formation de Bibliothèques Covalentes Dynamiques (BCDs). Cependant, l’interconversion entre des dérivées Knoevenagel de l’acide diméthylbarbiturique et des imines se déroule rapidement sans catalyseur. Une nouvelle classe de CCD basée sur des échanges par substitutions nucléophiles (SN2/SN2’) entre des sels d’ammonium quaternaires et des amines tertiaires est développée, impliquant la catalyse par l’iodure. Les réa

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18

Biggs, Timothy Nolen. "Part I. Thermal and photochemical rearrangements of p-quinol cyclopropyl ethers to spiro-fused tetralones. Part II. Preparation and reactivity of p-benzoquinol imines. Investigation of glutathione/quinol imine coupling and quinol... /." The Ohio State University, 1994. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487849696967873.

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19

Andrus, Danice M. "The design and synthesis of imine-bridged cyclic peptides andthe solid phase synthesis of β-turn mimetics". Thesis, The University of Arizona, 2004. http://hdl.handle.net/10150/291597.

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Pain is perhaps the most unpleasant sensation humans experience. While pain is important in preventing further injury and as a detection mechanism for ill-health; effective relief of pain, especially chronic or neuropathic, is a critical quality of life issue. As discoveries are made regarding opioid receptor-acceptor-ligand interactions, ligands that bind specifically to a receptor subtype can modify behavior without triggering side effects. Topographical space control is an important consideration in ligand design. According to Ramachandran¹, α-amino acids are confined to the following low-e

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20

Youtsler, Taylor Andrew. "Conjugation Studies: The Synthesis of Vinyl Aziridines through the aza-Darzens Reaction." Thesis, The University of Arizona, 2015. http://hdl.handle.net/10150/596123.

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Aziridines, three membered heterocycles containing a nitrogen in the ring, are extremely valuable to synthetic organic chemistry, as subjecting these compounds to ring opening processes initiates further capabilities for the molecule. Additionally, aziridines themselves possess the capacity and characteristics suitable for pharmaceutical applications, increasing the interest and appeal for their synthesis. One of the approaches to the formation of these products is the aza-Darzens reaction between imines and brominated nucleophiles. The research presented here aims to analyze this technique, s

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21

Lowe, Jared M. "Synthesis and Characterization of Rhodium Acetate with Functionalized Benzonitriles." Digital Commons @ East Tennessee State University, 2015. https://dc.etsu.edu/honors/282.

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Dirhodium complexes are effective catalysts in carbene transformations. These reactions involve chemistry between the catalyst and a carbene generated in situ. In order to better understand the rhodium-carbon bond, studies of rhodium acetate, Rh2(OAc)4, and a variety of functionalized benzonitriles were proposed. Diadducts of rhodium acetate with 4-nitrobenzonitrile, 4-aminobenzonitrile, 4-(dimethylamino)benzonitrile, and 3,5-dinitrobenzonitrile were successfully prepared and characterized by X-ray crystallography. IR and NMR spectroscopy were also employed for characterization purposes.

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22

Lafrance, Danny. "Investigations of metal carbonyl complexes as potential catalysts for the alternating co-polymerization of imine and CO into polypeptides." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1999. http://www.collectionscanada.ca/obj/s4/f2/dsk1/tape7/PQDD_0020/MQ55073.pdf.

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23

Chou, Chun-Tzer. "Part I, reaction of quinone imine monoketals with organolithium reagents. ; Part II, preparation of quinone imide monoketals by anodic oxidation of anilides. ; Part III, construction of the erythrina alkaloids skeleton /." The Ohio State University, 1987. http://rave.ohiolink.edu/etdc/view?acc_num=osu14875846121632.

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24

Holub, Jan. "Generation of coordination architectures from dynamic covalent ligand libraries." Thesis, Strasbourg, 2016. http://www.theses.fr/2016STRAF060/document.

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La Chimie Dynamique Combinatoire basée sur les liaisions imines (-C=N-), avec l’aide de la chimie de coordination, donne accès à différentes types d’architectures metallosupramoléculaires et de réseaux dynamiques fonctionnels. Le travail effectué au cours de cette thèse traite de ces deux aspects. Dans un premier temps des structures de types grilles moléculaire et de type hélicate ont été synthétisés, à l’aide de métaux donnant une coordination octahédrale ou tétraédrale, et leurs propriétés dans un environnement dynamique ont été étudiées. Dans un deuxième temps des réseaux dynamiques, prése

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25

Ren, Fengfeng. "Dynamic Covalent Self-Assembly of 2- and 3-Tiered Stacks." Miami University / OhioLINK, 2018. http://rave.ohiolink.edu/etdc/view?acc_num=miami1515171393581691.

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26

Lutz, Eric. "Dynamic covalent surfactants for the controlled release of bioactive volatiles." Thesis, Strasbourg, 2014. http://www.theses.fr/2014STRAF041/document.

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Ce projet consiste à fabriquer et à étudier des micelles à la fois biocompatibles et capables de relarguer des molécules volatiles bioactives à partir d’une solution aqueuse sous l’influence de stimuli extérieurs tel que le pH, la température ou la concentration. Pour atteindre ce but, nous avons étudiés un nouveau type d’objets micellaires qui sont formés par l’auto-assemblage d’amphiphiles covalents dynamiques (DCAs), des surfactants peu onéreux formés de l’association moléculaire réversible d’un bloc hydrophile et d’un bloc hydrophobe. Ces systèmes peuvent relarger une large gamme de fragra

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27

Larson, Shawn E. "Enantioselective Brønsted and Lewis Acid-Catalyzed Reaction Methodology: Aziridines as Building Blocks for Catalytic Asymmetric Induction." Scholar Commons, 2012. http://scholarcommons.usf.edu/etd/4357.

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Chiral molecules as with biological activity are plentiful in nature and the chemical literature; however they represent a smaller portion of the pharmaceutical drug market. As asymmetric methodologies grow more powerful, the tools are becoming available to synthesize chiral molecules in an enantioselective and efficient manner. Recent breakthroughs in our understanding of phosphoric acid now allow for Lewis acid catalysis via pairing with alkaline earth metals. Using alkaline earth metals with chiral phosphates is an emerging approach to asymmetric methodology, but already has an influential

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28

Zanirati, Stefano. "Synthesis and nanostructuring modulations of self-assembled dynamic covalent amphiphiles." Thesis, Strasbourg, 2013. http://www.theses.fr/2013STRAF039.

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Contrôler les forces supramoléculaires et chirales a toujours été un défi pour la communauté scientifique. Dynablocks sont amphiphile basés sur des liaisons covalentes réversibles (imine) qui, dans l’eau, s’auto–assemblent en mésophases. Avec un nouveaux aldéhydes chargés et avec divers types d'amines (pKa et chaînes de PEG variables) dynablocks chargées ont été utilisés pour ajuster les surfaces micellaires (inversion noyau/coquille). Nous avons également étudié les propriétésd'auto-réplication (autopoiesis) et leur intérêt pour les premiers réplicateurs de la Terre prébiotique. Dynablocks no

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29

MERCALLI, VALENTINA. "Nitrile N-oxides and nitrile imines as electrophilic partners for the discovery of novel isocyanide multicomponent reactions: an innovative strategy for the synthesis of molecular scaffolds useful in medicinal chemistry." Doctoral thesis, Università del Piemonte Orientale, 2017. http://hdl.handle.net/11579/86920.

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30

Kandappa, Sunil Kumar. "Light as a Reagent for Chemical Reactions-Excited State Manipulation to Discover New Reactivity." Bowling Green State University / OhioLINK, 2019. http://rave.ohiolink.edu/etdc/view?acc_num=bgsu1573830383912829.

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31

Gunler, Zeynep Inci. "Synthesis Of N-(2-propylphenyl) Substituted Chiral Amino Alcohols And Their Usage In Enantioselective Diethylzinc Addition Reactions." Master's thesis, METU, 2011. http://etd.lib.metu.edu.tr/upload/12613001/index.pdf.

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Chiral 1,2-amino alcohols were synthesized via newly developed &ldquo<br>intramolecular unsaturation transfer&rdquo<br>using cyclohexanone, propargyl bromide, and various chiral amino alcohols as starting components. These amino alcohols can be potential chiral ligands for many asymmetric transformation reactions. Therefore, their effectiveness as chiral ligands in diethylzinc addition to benzaldehyde and N-diphenylphosphinoyl imines were tested. Various parameters including temperature, solvent, ligand amount etc. were screened for the synthesized chiral ligands. In diethylzinc addition to be

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32

Barner, Claudia Jane. "Part I. Coordination chemistry of high-valent osmium polyanionic chelating ligand complexes with imine, imido and nitrido ligands. : Part II. Asymmetric hydrogenation using a resolved chiral scandium hydride complex /." Diss., Pasadena, Calif. : California Institute of Technology, 1990. http://resolver.caltech.edu/CaltechETD:etd-06112007-095040.

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33

Dhakal, Ram Chandra. "New Approaches To Heterocycle Synthesis: A Greener Route To Structurally Complex Protonated Azomethine Imines, And Their Use In 1,3-Dipolar Cycloadditions." ScholarWorks @ UVM, 2017. http://scholarworks.uvm.edu/graddis/777.

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1-Aza-2-azoniaallene salts are reactive intermediates that undergo [3+2] cycloaddition with many different types of multiple bonds. For the past several years, the Brewer group has studied the reactivity of these intermediates in intramolecular reactions, and have discovered that these cationic heteroallenes can react through a variety of other, mechanistically distinct, pathways to give different classes of nitrogen heterocycles. For example, prior work in the Brewer group revealed that 1-aza-2-azoniaallene salts could react in an intramolecular [4+2] cycloaddition reaction to give protonated

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34

Trifonova, Anna. "Synthesis of Novel Chiral Bicyclic Ligands and their Application in Iridium-Catalyzed Reactions." Doctoral thesis, Uppsala : Acta Universitatis Upsaliensis, 2005. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-5783.

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35

Arefalk, Anna. "New Methods for the Synthesis of 3-Substituted 1-Indanones : A Palladium-Catalyzed Approach." Doctoral thesis, Uppsala : Acta Universitatis Upsaliensis : Univ.-bibl. [distributör], 2005. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-6015.

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36

Capra, Julien. "Synthèse biomimétique de composés azotés biologiquement actifs." Phd thesis, Université Paris Sud - Paris XI, 2011. http://tel.archives-ouvertes.fr/tel-00711703.

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Ce travail de thèse est consacré à la synthèse de composés azotés biologiquement actifs s'inspirant notamment d'une réaction biosynthétique. Dans un premier temps, nos travaux avaient pour but de développer une nouvelle voie d'accès aux acides α-aminés par une réaction d'isomérisation énantiosélective d'imines. Après différentes études préliminaires, les meilleurs précurseurs d'acides a-aminés par cette méthode que nous ayons identifiés sont les α-céto amides. L'isomérisation 1,3 d'une imine formée à partir d'un α-céto amide et de la diphénylméthanamine à l'aide de différents alcoolates chirau

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37

Tanh, Jeazet Harold Brice. "Metallo-supramolecular Architectures based on Multifunctional N-Donor Ligands." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2010. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-39665.

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Self-assembly processes were used to construct supramolecular architectures based on metal-ligand interactions. The structures formed strongly depend on the used metal ion, the ligand type, the chosen counter ion and solvent as well as on the experimental conditions. The focus of the studies was the design of multifunctional N-donor ligands and the characterization of their complexing and structural properties. This work was divided into three distinct main parts: The bis(2-pyridylimine), the bis(2-hydroxyaryl) imine and the tripodal imine / amine ligand approach. In the first part a series o

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38

Jurca, Titel. "Charting New Territory in Bis(imino)pyridine Coordination Chemistry." Thèse, Université d'Ottawa / University of Ottawa, 2012. http://hdl.handle.net/10393/23089.

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This work was initially launched to study the synthesis of low-valent group 13 compounds bearing the bis(imino)pyridine ligand framework. Since its inception, this project has grown beyond the boundaries of group 13 to include low valent tin, silver, and rhenium. Alongside the reports of novel coordination compounds, we utilized computational chemistry to uncover unprecedented interactions which challenge conventional concepts of bonding. Synthesis, characterization, and complimentary computational studies are presented herein. Chapter 1 presents a historical overview of the bis(imino)pyridine

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39

Young, Adrian R. "Free radical cyclisation of imines." Thesis, Loughborough University, 1996. https://dspace.lboro.ac.uk/2134/15357.

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Introduction. The free radical cyclisation reaction onto an unsaturated bond is a well known synthetic pathway, where a wide range of cyclic compounds can be produced form acyclic starting materials. Up until recent years, free radical addition to multiple bonds other than carbon-carbon had been little studied. Nowadays there is much information available of radical addition to carbonyl, thiocarbonyl, nitrile and oxime ether (C=NOR) functional groups. However there has been surprisingly little detailed study of similar reactions involving imines (C=NR) or hydrazones (C=NNHR). Monocyclisation.

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40

Heaney, Mary Frances Teresa. "Cycloaddition reactions of oximes and imines." Thesis, Queen's University Belfast, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.335415.

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41

Alhalafi, Mona Hanash A. "Pyridone-substituted pyridyl imines as functionalised ligands in coordination chemistry and catalysis." Thesis, University of Leicester, 2018. http://hdl.handle.net/2381/42404.

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In this thesis, the synthesis and coordination chemistry of a series of novel NNN and NN proton responsive ligands are described. All the ligands and complexes have been characterized by a combination of multinuclear NMR spectroscopic techniques, mass spectrometry, IR spectroscopy and by single crystal X-ray diffraction studies. Chapter 1 presents an introduction to functional ligands/complexes and their applications in catalysis. In Chapter 2, the synthesis and characterisation of a series of OH-functionalised NNN pincer ligands are discussed. The coordination chemistry of these pyridone-subs

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42

Hartley, James Holroyd. "Saccharide accelerated hydrolysis of boronic acid imines." Thesis, University of Birmingham, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.369335.

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43

Vrankova, Kvetoslava. "Scope of enantioselective reduction of imines with trichlorosilane." Thesis, University of Glasgow, 2009. http://theses.gla.ac.uk/1390/.

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Herein, we report the results of research continuing previous successI in the field of enantioselective organocatalytic reduction of imines with trichlorosilane. Syntheses of various precursors (ketones) and substrates (imines) for the reduction reaction and their reduction following the protocol (Scheme A1) are described in this thesis. 1. Aromatic heterocycles containing nitrogen – good yields of the reduced product (68-85 %), the enantioselectivity depended on steric bulk in proximity to the nitrogen, steric bulk improved the enantioselectivity (up to 78 % ee), probably due to thwarting the

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44

Warnock, William James. "1,3-dipolar cycloaddition reactions of imines and oximes." Thesis, Queen's University Belfast, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.356974.

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45

Mitchell, S. H. "Structural studies on some complex compounds containing imines." Thesis, Cardiff University, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.332450.

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46

Barr, Darrin Alexander. "Metal catalysed cycloadditions of imines of #alpha#-amino esters." Thesis, Queen's University Belfast, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.334558.

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47

Smith, David F. "Applications of the imino Diels-Alder reaction in synthesis." Thesis, University of Cambridge, 1992. https://www.repository.cam.ac.uk/handle/1810/272878.

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48

Shtaiwi, Majed Hamad Mohammad Attari Shtaiwi. "Iminopropadienones syntheses and reations /." St. Lucia, Qld, 2002. http://www.library.uq.edu.au/pdfserve.php?image=thesisabs/absthe16440.pdf.

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49

Smith, Joshua J. "Stereoselective Rh- and Cu-catalysed additions to imines and aldehydes." Thesis, University of Nottingham, 2017. http://eprints.nottingham.ac.uk/39370/.

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Chapter 1.Copper-Catalysed Borylative Coupling of Vinylazaarenes and N-Boc Imines. Methodology for the copper-catalysed three-component couplings of vinylazaarenes, bis(pinacolato)diboron, and N-Boc imines has been developed. Oxidation of the initially formed boron species gives azaarene-containing, Boc-protected amino alcohols with reasonable to good diastereoselectivities. Additionally the synthetic utility of the reaction products have been demonstrated. The crude boron species have been shown to undergo a Suzuki-Miyaura cross coupling to give further functionalised products. Finally, facil

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50

Power, Nicholas Patrick. "Kinetics and mechanisms of reactions of N-arylsulfonyl derivatives of imines." Thesis, University of Ulster, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.267781.

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