Academic literature on the topic 'Microwave assisted synthesis route'

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Journal articles on the topic "Microwave assisted synthesis route"

1

Yu, Siming, Jordan A. Hachtel, Matthew F. Chisholm, Sokrates T. Pantelides, Anna Laromaine, and Anna Roig. "Magnetic gold nanotriangles by microwave-assisted polyol synthesis." Nanoscale 7, no. 33 (2015): 14039–46. http://dx.doi.org/10.1039/c5nr03113c.

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2

Ahn, Jong Bin, Dong Soo Kim, Young Kook Kim, and Jung Goo Lee. "Synthesis of AlN Particles by Microwave-Assisted Urea Route." Applied Mechanics and Materials 851 (August 2016): 191–95. http://dx.doi.org/10.4028/www.scientific.net/amm.851.191.

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Novel simple route to prepare AlN nanoparticles was proposed in this study. Aluminum nitride powder was synthesized by microwave-assisted urea route. Aluminum chloride was dissolved in ethanol and urea was added to this solution considering molar concentration with Aluminum chloride. The solution was heated under microwave (MW) irradiation from 60°C to 80°C for 5-10 minutes. And then heat treatment was performed in N2 atmosphere with various temperatures and time to obtain AlN particles. While microwave was irradiated to the mixed solution with Aluminum chloride, urea and ethanol, the solvent
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3

Tyrrell, Sophie, Gereon Behrendt, Yawen Liu, and Peter Nockemann. "Zinc selenide nano- and microspheres via microwave-assisted ionothermal synthesis." RSC Adv. 4, no. 68 (2014): 36110–16. http://dx.doi.org/10.1039/c4ra06883a.

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4

Panneerselvam, M., G. N. Subanna, and K. J. Rao. "Translucent yttrium aluminum garnet: Microwave-assisted route to synthesis and processing." Journal of Materials Research 16, no. 10 (2001): 2773–76. http://dx.doi.org/10.1557/jmr.2001.0379.

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A novel and fast microwave route is described for the synthesis of yttrium aluminum garnet (YAG) and for its sintering to translucent bodies. Precursor was made by microwave decomposition (20 min) of aluminum tri-sec-butoxide and yttrium nitrate dissolved in ethyl acetate. The precursor, conventionally calcined at 1000 °C (1 h), was sintered in microwave using SiC as secondary heater for just 35 min. Resulting translucent YAG has a microhardness (HV) of 18.1 GPa and fracture toughness (KIC) of 4.3 MPa m1/2. A 0.86-mm-thick sintered pellet exhibits approximately 45% transmission for 520-nm radi
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Lagashetty, Arunkumar, Vijayanand Havanoor, S. Basavaraja, S. D. Balaji, and A. Venkataraman. "Microwave-assisted route for synthesis of nanosized metal oxides." Science and Technology of Advanced Materials 8, no. 6 (2007): 484–93. http://dx.doi.org/10.1016/j.stam.2007.07.001.

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6

Polshettiwar, Vivek, Mallikarjuna N. Nadagouda, and Rajender S. Varma. "Microwave-Assisted Chemistry: a Rapid and Sustainable Route to Synthesis of Organics and Nanomaterials." Australian Journal of Chemistry 62, no. 1 (2009): 16. http://dx.doi.org/10.1071/ch08404.

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The use of emerging microwave (MW)-assisted chemistry techniques in conjunction with benign reaction media is dramatically reducing chemical waste and reaction times in several organic syntheses and chemical transformations. The present review summarizes recent developments in MW-assisted synthesis, name reactions and organic transformations, and rapid generation of nanoparticles with uniform size distribution. Greener protocols have been developed for the synthesis of various bio-active heterocycles, namely 1,3,4-oxadiazoles, 1,3,4-thiadiazoles, 1,3-dioxanes, pyrazoles, hydrazones and 3,4-dih
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Jung, Young Mi, та Sang Woo Kim. "Microwave-Assisted Combustion Synthesis of α-Alumina and Magnesium Aluminate Spinel Nanocomposite Powders". Solid State Phenomena 119 (січень 2007): 191–94. http://dx.doi.org/10.4028/www.scientific.net/ssp.119.191.

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Microwave-assisted combustion synthesis of α-alumina-magnesium spinel nanocomposite powders from a route using ammonium aluminum carbonate hydroxide (AACH) as a precursor was studied. γ- to α-phase transformation temperature of microwave-assisted alumina composite powders is lowered by 100°C compared to that of normal heat-treated alumina composite powders. The crystallite size of the microwave-assisted composite powders was considerably decreased from 42 nm to 29 nm compared to that of the normal heat treated composite powders. Nanosized α- alumina-magnesium aluminate composite powders were s
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8

Jalota, Sahil, A. Cuneyt Tas, and Sarit B. Bhaduri. "Microwave-assisted synthesis of calcium phosphate nanowhiskers." Journal of Materials Research 19, no. 6 (2004): 1876–81. http://dx.doi.org/10.1557/jmr.2004.0230.

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Calcium phosphate [single-phase hydroxyapatite (HA), single-phase tricalcium phosphate (TCP), and biphasic HA-TCP] nanowhiskers and/or powders were produced by using a novel microwave-assisted “combustion synthesis (auto ignition)/molten salt synthesis” hybrid route. This work is an example of our “synergistic processing” philosophy combining these three technologies while taking advantage of their useful aspects. Aqueous solutions containing NaNO3, Ca(NO3)2·4H2O and KH2PO4 (with or without urea) were irradiated in a household microwave oven for 5 min at 600 watts of power. The as-synthesized
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Pérez-Escalante, Emmanuel, Luis Guillermo González-Olivares, Araceli Castañeda-Ovando, et al. "Green, Microwave-Assisted Synthesis of O-Perbutyrylated-Alkyl-Glycosides." Proceedings 41, no. 1 (2019): 42. http://dx.doi.org/10.3390/ecsoc-23-06500.

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Chemical synthesis of carbohydrates is a challenging task. Several protection and deprotection steps of hydroxyl groups are required to ensure regioselective formation of the glycosidic bond. Usually, it is achieved through acylation, where conventional heating is combined with addition of Lewis acids as catalysts. This traditional approach has two drawbacks; it is time consuming and often catalysts are hazardous to the environment. An alternative route relies on application of microwaves and/or other Lewis acids with less or no toxicity. Such combination would reduce reaction times and offer
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10

Bozinovic, Nina, Bogdan Solaja, and Igor Opsenica. "Microwave-assisted synthesis of azepines via nucleophilic aromatic substitution." Journal of the Serbian Chemical Society 81, no. 11 (2016): 1225–30. http://dx.doi.org/10.2298/jsc160824074b.

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A novel and efficient route has been developed to afford 5H-dipyridoazepine derivatives from primary amines and 3,3'-(Z)-ethene-1,2-di-ylbis(4-chloropyridine). The procedure based on the double nucleophilic aromatic substitution provides a valuable synthetic tool for the synthesis of dipyridoazepines. The reaction proceeds without catalyst, under microwave irradiation condition.
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