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Journal articles on the topic 'Microwave assisted synthesis route'

Author: Grafiati

Published: 4 June 2021

Last updated: 2 February 2022

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1

Yu, Siming, Jordan A. Hachtel, Matthew F. Chisholm, Sokrates T. Pantelides, Anna Laromaine, and Anna Roig. "Magnetic gold nanotriangles by microwave-assisted polyol synthesis." Nanoscale 7, no. 33 (2015): 14039–46. http://dx.doi.org/10.1039/c5nr03113c.

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2

Ahn, Jong Bin, Dong Soo Kim, Young Kook Kim, and Jung Goo Lee. "Synthesis of AlN Particles by Microwave-Assisted Urea Route." Applied Mechanics and Materials 851 (August 2016): 191–95. http://dx.doi.org/10.4028/www.scientific.net/amm.851.191.

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Novel simple route to prepare AlN nanoparticles was proposed in this study. Aluminum nitride powder was synthesized by microwave-assisted urea route. Aluminum chloride was dissolved in ethanol and urea was added to this solution considering molar concentration with Aluminum chloride. The solution was heated under microwave (MW) irradiation from 60°C to 80°C for 5-10 minutes. And then heat treatment was performed in N2 atmosphere with various temperatures and time to obtain AlN particles. While microwave was irradiated to the mixed solution with Aluminum chloride, urea and ethanol, the solvent

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3

Tyrrell, Sophie, Gereon Behrendt, Yawen Liu, and Peter Nockemann. "Zinc selenide nano- and microspheres via microwave-assisted ionothermal synthesis." RSC Adv. 4, no. 68 (2014): 36110–16. http://dx.doi.org/10.1039/c4ra06883a.

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4

Panneerselvam, M., G. N. Subanna, and K. J. Rao. "Translucent yttrium aluminum garnet: Microwave-assisted route to synthesis and processing." Journal of Materials Research 16, no. 10 (2001): 2773–76. http://dx.doi.org/10.1557/jmr.2001.0379.

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A novel and fast microwave route is described for the synthesis of yttrium aluminum garnet (YAG) and for its sintering to translucent bodies. Precursor was made by microwave decomposition (20 min) of aluminum tri-sec-butoxide and yttrium nitrate dissolved in ethyl acetate. The precursor, conventionally calcined at 1000 °C (1 h), was sintered in microwave using SiC as secondary heater for just 35 min. Resulting translucent YAG has a microhardness (HV) of 18.1 GPa and fracture toughness (KIC) of 4.3 MPa m1/2. A 0.86-mm-thick sintered pellet exhibits approximately 45% transmission for 520-nm radi

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5

Lagashetty, Arunkumar, Vijayanand Havanoor, S. Basavaraja, S. D. Balaji, and A. Venkataraman. "Microwave-assisted route for synthesis of nanosized metal oxides." Science and Technology of Advanced Materials 8, no. 6 (2007): 484–93. http://dx.doi.org/10.1016/j.stam.2007.07.001.

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6

Polshettiwar, Vivek, Mallikarjuna N. Nadagouda, and Rajender S. Varma. "Microwave-Assisted Chemistry: a Rapid and Sustainable Route to Synthesis of Organics and Nanomaterials." Australian Journal of Chemistry 62, no. 1 (2009): 16. http://dx.doi.org/10.1071/ch08404.

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The use of emerging microwave (MW)-assisted chemistry techniques in conjunction with benign reaction media is dramatically reducing chemical waste and reaction times in several organic syntheses and chemical transformations. The present review summarizes recent developments in MW-assisted synthesis, name reactions and organic transformations, and rapid generation of nanoparticles with uniform size distribution. Greener protocols have been developed for the synthesis of various bio-active heterocycles, namely 1,3,4-oxadiazoles, 1,3,4-thiadiazoles, 1,3-dioxanes, pyrazoles, hydrazones and 3,4-dih

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7

Jung, Young Mi, та Sang Woo Kim. "Microwave-Assisted Combustion Synthesis of α-Alumina and Magnesium Aluminate Spinel Nanocomposite Powders". Solid State Phenomena 119 (січень 2007): 191–94. http://dx.doi.org/10.4028/www.scientific.net/ssp.119.191.

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Microwave-assisted combustion synthesis of α-alumina-magnesium spinel nanocomposite powders from a route using ammonium aluminum carbonate hydroxide (AACH) as a precursor was studied. γ- to α-phase transformation temperature of microwave-assisted alumina composite powders is lowered by 100°C compared to that of normal heat-treated alumina composite powders. The crystallite size of the microwave-assisted composite powders was considerably decreased from 42 nm to 29 nm compared to that of the normal heat treated composite powders. Nanosized α- alumina-magnesium aluminate composite powders were s

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8

Jalota, Sahil, A. Cuneyt Tas, and Sarit B. Bhaduri. "Microwave-assisted synthesis of calcium phosphate nanowhiskers." Journal of Materials Research 19, no. 6 (2004): 1876–81. http://dx.doi.org/10.1557/jmr.2004.0230.

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Calcium phosphate [single-phase hydroxyapatite (HA), single-phase tricalcium phosphate (TCP), and biphasic HA-TCP] nanowhiskers and/or powders were produced by using a novel microwave-assisted “combustion synthesis (auto ignition)/molten salt synthesis” hybrid route. This work is an example of our “synergistic processing” philosophy combining these three technologies while taking advantage of their useful aspects. Aqueous solutions containing NaNO3, Ca(NO3)2·4H2O and KH2PO4 (with or without urea) were irradiated in a household microwave oven for 5 min at 600 watts of power. The as-synthesized

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9

Pérez-Escalante, Emmanuel, Luis Guillermo González-Olivares, Araceli Castañeda-Ovando, et al. "Green, Microwave-Assisted Synthesis of O-Perbutyrylated-Alkyl-Glycosides." Proceedings 41, no. 1 (2019): 42. http://dx.doi.org/10.3390/ecsoc-23-06500.

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Chemical synthesis of carbohydrates is a challenging task. Several protection and deprotection steps of hydroxyl groups are required to ensure regioselective formation of the glycosidic bond. Usually, it is achieved through acylation, where conventional heating is combined with addition of Lewis acids as catalysts. This traditional approach has two drawbacks; it is time consuming and often catalysts are hazardous to the environment. An alternative route relies on application of microwaves and/or other Lewis acids with less or no toxicity. Such combination would reduce reaction times and offer

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10

Bozinovic, Nina, Bogdan Solaja, and Igor Opsenica. "Microwave-assisted synthesis of azepines via nucleophilic aromatic substitution." Journal of the Serbian Chemical Society 81, no. 11 (2016): 1225–30. http://dx.doi.org/10.2298/jsc160824074b.

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A novel and efficient route has been developed to afford 5H-dipyridoazepine derivatives from primary amines and 3,3'-(Z)-ethene-1,2-di-ylbis(4-chloropyridine). The procedure based on the double nucleophilic aromatic substitution provides a valuable synthetic tool for the synthesis of dipyridoazepines. The reaction proceeds without catalyst, under microwave irradiation condition.

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11

Illanes Tormena, Renata Pascoal, Eliane Vieira Rosa, Bruna de Fátima Oliveira Mota, et al. "Evaluation of the antimicrobial activity of silver nanoparticles obtained by microwave-assisted green synthesis using Handroanthus impetiginosus (Mart. ex DC.) Mattos underbark extract." RSC Advances 10, no. 35 (2020): 20676–81. http://dx.doi.org/10.1039/d0ra03240a.

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12

Navaneethan, M., J. Archana, K. D. Nisha, et al. "Synthesis of wurtzite ZnS nanorods by microwave assisted chemical route." Materials Letters 66, no. 1 (2012): 276–79. http://dx.doi.org/10.1016/j.matlet.2011.08.082.

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13

Tanisan, Belgin, and Michele Dondi. "Cobalt chromite nano pigments synthesis through microwave-assisted polyol route." Journal of Sol-Gel Science and Technology 83, no. 3 (2017): 590–95. http://dx.doi.org/10.1007/s10971-017-4449-1.

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14

Ashton, Thomas E., David Hevia Borrás, Antonella Iadecola, et al. "Microwave-assisted synthesis and electrochemical evaluation of VO2 (B) nanostructures." Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials 71, no. 6 (2015): 722–26. http://dx.doi.org/10.1107/s2052520615021289.

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Understanding how intercalation materials change during electrochemical operation is paramount to optimizing their behaviour and function and in situ characterization methods allow us to observe these changes without sample destruction. Here we first report the improved intercalation properties of bronze phase vanadium dioxide VO2 (B) prepared by a microwave-assisted route which exhibits a larger electrochemical capacity (232 mAh g−1) compared with VO2 (B) prepared by a solvothermal route (197 mAh g−1). These electrochemical differences have also been followed using in situ X-ray absorption sp

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15

Baozhi, Li, Yang Gengliang, Zhang Jinsong, and Duan Kefang. "Microwave-Assisted Synthesis ofp[n]arene Catalyzed by KOH." E-Journal of Chemistry 2, no. 1 (2005): 70–74. http://dx.doi.org/10.1155/2005/470510.

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The paper researched the synthesis of p-methylcalix[6]arene and p-tertbutylcalix[8]arene catalyzed by KOH in moderate yields under microwave irradiation. The effects of different factors on this condensation reaction have been discussed. Compared with classical method, this method had some merits such as easy obtaining the raw materials, short reaction route, simple and convenient aftertreatment, being beneficial to environmental protection.

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16

Segmehl, Jana S., Anna Laromaine, Tobias Keplinger, Anna May-Masnou, Ingo Burgert, and Anna Roig. "Magnetic wood by in situ synthesis of iron oxide nanoparticles via a microwave-assisted route." Journal of Materials Chemistry C 6, no. 13 (2018): 3395–402. http://dx.doi.org/10.1039/c7tc05849g.

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17

Saha, Sonali, M. M. Malik, and M. S. Qureshi. "Microwave Synthesis of Silver Nanoparticles." Nano Hybrids 4 (May 2013): 99–112. http://dx.doi.org/10.4028/www.scientific.net/nh.4.99.

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In this work, a green route for synthesis of Ag nanoparticles is presensted. For the synthesis of Ag nanoparticles, tulasi leaf extract (Ocimum leaf) in combination with microwave irradiation was used which yielded stable spherical Ag nanoparticle in the range of 5-50 nm. Surface morphology of nanoparticle was analyzed by XRD and TEM. UV-Vis analysis was also carried out to characterize the synthesized nanoparticles. The main feature of the process is that it is carried out in a very short span of time in comparison to other conventional physical, chemical and biological methods. Microwave ass

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18

Novais, S. M. V., P. C. R. Silva, Z. S. Macedo, and L. B. Barbosa. "Short Time and Low Temperature Reaction between Metal Oxides through Microwave-Assisted Hydrothermal Method." Advances in Condensed Matter Physics 2016 (2016): 1–7. http://dx.doi.org/10.1155/2016/3745459.

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This work demonstrates the possibility of synthesis of cadmium tungstate at low temperatures using oxide precursors. Cadmium tungstate (CdWO4) scintillator was produced via microwave-assisted hydrothermal reaction using the precursors CdO and WO3. The methodology was based on microwave radiation for heating, which is remarkably faster than the solid-state route or conventional hydrothermal procedure. CdWO4 monoclinic (wolframite) structure was successfully obtained at 120°C for synthesis times as short as 20 min. This route does not require the use of templates or surfactants and yields self-a

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19

Zheng, Hangsong, Yonghong Ni, Fengying Wan, and Xiang Ma. "Fast synthesis and electrochemical performance of hollow NiCo2O4 flowerlike microstructures." RSC Advances 5, no. 40 (2015): 31558–65. http://dx.doi.org/10.1039/c5ra03747f.

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Hollow NiCo<sub>2</sub>O<sub>4</sub> flowerlike microstructures with good electrochemical performance were successfully prepared through a fast microwave-assisted hydrothermal route and sequential pyrolysis.

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20

Manna, Sudipta Kumar, and Gautam Panda. "Microwave assisted [RuCl2(p-cymene)2]2 catalyzed regioselective endo-tandem cyclization involving imine and alkyne activation: an approach to benzo[4,5]imidazo[2,1-a]pyridine scaffold." RSC Adv. 4, no. 40 (2014): 21032–41. http://dx.doi.org/10.1039/c4ra02581d.

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21

ROY, ARUP, and JAYANTA BHATTACHARYA. "MICROWAVE-ASSISTED SYNTHESIS AND CHARACTERIZATION OF CaS NANOPARTICLES." International Journal of Nanoscience 11, no. 05 (2012): 1250027. http://dx.doi.org/10.1142/s0219581x12500275.

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CaS nanoparticles have been synthesized by microwave irradiation, using Ca(Ac)2 as Ca -precursor, and thioacetamide as S -source. The as-prepared sample has a uniform morphology and high purity. After heat treatment similar results were observed. Synthesized nanoparticles were characterized by X-ray powder analysis (XRD), field emission scanning microscopy (FESEM), high resolution transmission electron microscopy (TEM), and UV-Vis absorption spectroscopy. X-ray diffraction patterns suggest the formation of single cubical face of CaS having average particle size of 22 nm. HRTEM micrographs reve

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22

Wixtrom, Alex I., Yanwu Shao, Dahee Jung, et al. "Rapid synthesis of redox-active dodecaborane B12(OR)12 clusters under ambient conditions." Inorganic Chemistry Frontiers 3, no. 5 (2016): 711–17. http://dx.doi.org/10.1039/c5qi00263j.

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We have developed a fast and efficient route to obtain perfunctionalized ether-linked alkyl and benzyl derivatives of the closo-[B<sub>12</sub>(OH)<sub>12</sub>]<sup>2−</sup> icosahedral dodecaborate cluster via microwave-assisted synthesis.

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23

Zhang, Lujun, Zhaofu Zhang, Congyi Wu, et al. "Microwave assisted synthesis of glycerol carbonate from glycerol and urea." Pure and Applied Chemistry 90, no. 1 (2018): 1–6. http://dx.doi.org/10.1515/pac-2017-0303.

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AbstractThe transformation of glycerol into value-added chemicals is an interesting topic in Green Chemistry. The glycerolysis of urea into glycerol carbonate is an important route of glycerol transformation. In this work, the synthesis of glycerol carbonate from glycerol and urea was performed under microwave irradiation and solvent free conditions. The catalytic properties of ZnSO4, ZnCl2, CuSO4 and MgSO4 were tested and ZnSO4 showed the best performance. The effects of catalyst amount, temperature, reaction time, microwave power, molar ratio of urea to glycerol on the reaction were studied

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24

Bu, Fanxing, Wenshu Chen, Mohamed F. Aly Aboud, Imran Shakir, Jiajun Gu, and Yuxi Xu. "Microwave-assisted ultrafast synthesis of adjustable bimetal phosphide/graphene heterostructures from MOFs for efficient electrochemical water splitting." Journal of Materials Chemistry A 7, no. 24 (2019): 14526–35. http://dx.doi.org/10.1039/c9ta03146d.

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25

Rizzuti, Anotnio, Massimo Viviani, Anna Corradi, Paolo Nanni, and Cristina Leonelli. "Microwave-Assisted Hydrothermal Synthesis as a Rapid Route Towards Manganite Preparation." Solid State Phenomena 128 (October 2007): 21–24. http://dx.doi.org/10.4028/www.scientific.net/ssp.128.21.

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In this work attempts to prepare strontium-doped lanthanum manganites La1-xSrxMnO3 using microwave-assisted hydrothermal synthesis were undertaken from a mixture of lanthanum nitrate, strontium nitrate, manganese(II) nitrate, potassium permanganate and potassium hydroxide as a mineralizer. For x = 0.3, and x = 0.5, the perovskite obtained is not defined since both La0.7Sr0.3MnO3 and La0.5Sr0.5MnO3 phases are consistent with XRD spectra. While with x = 1.0, for the first time, hexagonal strontium manganite was prepared as blade-shaped crystallites with a narrow particle length distribution (ran

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26

Long, Fei, Shuyi Mo, Yan Zeng, Shangsen Chi, and Zhengguang Zou. "Synthesis of Flower-Like Cu2ZnSnS4Nanoflakes via a Microwave-Assisted Solvothermal Route." International Journal of Photoenergy 2014 (2014): 1–4. http://dx.doi.org/10.1155/2014/618789.

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Flower-like Cu2ZnSnS4(CZTS) nanoflakes were synthesized by a facile and fast one-pot solution reaction using copper(II) acetate monohydrate, zinc acetate dihydrate, tin(IV) chloride pentahydrate, and thiourea as starting materials. The as-synthesized samples were characterized by X-ray diffraction (XRD), Raman scattering analysis, field emission scanning electron microscopy (FESEM) equipped with an energy dispersion X-ray spectrometer (EDS), transmission electron microscopy (TEM), and UV-Vis absorption spectra. The XRD patterns shown that the as-synthesized particles were kesterite CZTS and Ra

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27

Ghosh, Srabanti, Prasenjit Kar, Nimai Bhandary, et al. "Microwave-assisted synthesis of porous Mn2O3 nanoballs as bifunctional electrocatalyst for oxygen reduction and evolution reaction." Catalysis Science & Technology 6, no. 5 (2016): 1417–29. http://dx.doi.org/10.1039/c5cy01264c.

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28

Castillo, Juan-Carlos, Hernán-Alejandro Rosero, and Jaime Portilla. "Simple access toward 3-halo- and 3-nitro-pyrazolo[1,5-a]pyrimidines through a one-pot sequence." RSC Advances 7, no. 45 (2017): 28483–88. http://dx.doi.org/10.1039/c7ra04336h.

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Herein, a regioselective, time-efficient and one-pot route for the synthesis of diversely substituted 3-halo- and 3-nitropyrazolo[1,5-a]pyrimidines in good to excellent yields through a microwave-assisted process is provided.

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29

Dong, Li Min, Zhi Dong Han, Ze Wu, and Xian You Zhang. "Microwave-Assisted Synthesis of Hexagonal Barium Ferrite Powders with Nano-Particle." Key Engineering Materials 368-372 (February 2008): 576–78. http://dx.doi.org/10.4028/www.scientific.net/kem.368-372.576.

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A novel ceramic synthesis technique, microwave-assisted process was investigated for the production of Barium Hexagonal ferrite (BaFe12O19) powders with improved physical properties. Compared to conventional syntheticroute, the new method significantly shortened synthetic steps and reaction time. This technique involves the reaction of stoichiometric amount of metal nitrates and appropriate dosage of citric acid at microwave oven and the whole process took only 15 min. The powders of BaFe12O19 were further investigated by X-ray diffractometer (XRD) and scanning electron microscopy (SEM). The r

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30

Jung, Young Mi, та Sang Woo Kim. "Rapid Transformation of α-Alumina Nanocomposite Powders by Microwave Assisted Combustion". Solid State Phenomena 124-126 (червень 2007): 823–26. http://dx.doi.org/10.4028/www.scientific.net/ssp.124-126.823.

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The microwave-assisted combustion synthesis as a route to obtain ultrafine α-alumina and magnesium aluminate composite powders starting from the ammonium aluminum carbonate hydroxide precursor was investigated. The synthetic temperature and the crystallite size of the α- alumina nanocomposite powder were significantly affected by the environmental atmosphere in the microwave assisted combustion. The α-alumina and spinel composite powder was obtained by the microwave-assisted combustion at temperature of 1000°C under H2/N2, but at 1150°C by the normal heat process under air. The rapid transform

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31

Rao, Ramdas Nishanth, and Kaushik Chanda. "An expeditious microwave assisted one-pot sequential route to pyrido fused imidazo[4,5-c] quinolines in green media." New Journal of Chemistry 45, no. 6 (2021): 3280–89. http://dx.doi.org/10.1039/d0nj05835a.

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A novel one-pot sequential route for the synthesis of pyrido[2′,1′:2,3]imidazo[4,5-c]quinolines via microwave-assisted sequential reaction of 2-aminopyridines, 2-bromophenacyl bromides, and aldehydes has been developed in green media.

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32

Heilmann, Maria, Hannes Kulla, Carsten Prinz, et al. "Advances in Nickel Nanoparticle Synthesis via Oleylamine Route." Nanomaterials 10, no. 4 (2020): 713. http://dx.doi.org/10.3390/nano10040713.

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Nickel nanoparticles are an active research area due to their multiple applications as catalysts in different processes. A variety of preparation techniques have been reported for the synthesis of these nanoparticles, including solvothermal, microwave-assisted, and emulsion techniques. The well-studied solvothermal oleylamine synthesis route comes with the drawback of needing standard air-free techniques and often space-consuming glassware. Here, we present a facile and straightforward synthesis method for size-controlled highly monodisperse nickel nanoparticles avoiding the use of, e.g., Schl

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33

Praneeth, N. V. S., and Santanu Paria. "Microwave-assisted one-pot synthesis of anisotropic gold nanoparticles with active high-energy facets for enhanced catalytic and metal enhanced fluorescence activities." CrystEngComm 20, no. 30 (2018): 4297–304. http://dx.doi.org/10.1039/c8ce00654g.

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34

Joseph, Aswathy, Marylin Mary Xavier, Jacek Fal, et al. "Synthesis and electrochemical characterization of electroactive IoNanofluids with high dielectric constants from hydrated ferrous sulphate." Chemical Communications 55, no. 1 (2019): 83–86. http://dx.doi.org/10.1039/c8cc08243j.

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An iron oxide based-electroactive IoNanofluid with a high dielectric constant, high stability and low viscosity was synthesized from ferrous sulphate heptahydrate via a facile microwave assisted one-step route in 1-butyl-4-methylpyridinium chloride.

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35

Bhattacharjee, Archita, and M. Ahmaruzzaman. "CuO nanostructures: facile synthesis and applications for enhanced photodegradation of organic compounds and reduction of p-nitrophenol from aqueous phase." RSC Advances 6, no. 47 (2016): 41348–63. http://dx.doi.org/10.1039/c6ra03624d.

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36

WANG, JIAN-DONG, CHONG-XIAO LUO, JIN-KU LIU, YI LU, and GUANG-MING LI. "SYNTHESIS OF YTTRIA-STABILIZED CUBIC ZIRCONIA NANOCRYSTALS BY ULTRASONIC–MICROWAVE ROUTE." Nano 05, no. 05 (2010): 271–77. http://dx.doi.org/10.1142/s1793292010002177.

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The yttria-stabilized zirconia (YSZ) nanocrystals with uniform size, high purity, and high degree of crystallinity, were prepared by ultrasonic–microwave-assisted method. The structure, optical properties and morphologies of YSZ nanocrystals were characterized by X-ray powder diffraction (XRD), Raman spectroscopy, UV–vis absorption, scanning electron microscope (SEM) and transmission electron microscopy (TEM). The SEM and TEM images of the YSZ nanocrystals indicate that the product is a mono-dispersion structure with an average particle size of about 25 nm.

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Loveleenpreet Kaur and Gupta G D. "Gum colocasia-g-polyacrylamide: Microwave-assisted synthesis and characterization." International Journal of Research in Pharmaceutical Sciences 11, no. 4 (2020): 6698–706. http://dx.doi.org/10.26452/ijrps.v11i4.3595.

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In the present investigation, an attempt has been made for grafting of acrylamide on the backbone of Colocasia esculenta by using microwave-assisted grafting method, which is a convenient and versatile route for the development of polysaccharide-based materials. The dried mucilage of colocasia was prepared from fresh rhizomes. The optimization was performed by using Box Behnken matrix design (BBD) and response surface methodology (RSM) using design expert software. A series of graft polymers, varying in the amount of acrylamide, ammonium persulphate and microwave irradiation was prepared. The

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38

Parhi, Purnendu, A. Ramanan, and Alok R. Ray. "Synthesis of nano-sized alkaline-earth hydroxyapatites through microwave assisted metathesis route." Materials Letters 60, no. 2 (2006): 218–21. http://dx.doi.org/10.1016/j.matlet.2005.08.019.

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39

Wei, Pengfei, Xiangxue Zhu, Yanan Wang, et al. "Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route." Microporous and Mesoporous Materials 279 (May 2019): 220–27. http://dx.doi.org/10.1016/j.micromeso.2018.12.036.

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40

Sertkol, M., Y. Köseoğlu, A. Baykal, H. Kavas, and M. S. Toprak. "Synthesis and magnetic characterization of Zn0.7Ni0.3Fe2O4 nanoparticles via microwave-assisted combustion route." Journal of Magnetism and Magnetic Materials 322, no. 7 (2010): 866–71. http://dx.doi.org/10.1016/j.jmmm.2009.11.018.

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41

Wu, Zhengcui, Mingwang Shao, Wu Zhang, and Youbao Ni. "Large-scale synthesis of uniform Cu2O stellar crystals via microwave-assisted route." Journal of Crystal Growth 260, no. 3-4 (2004): 490–93. http://dx.doi.org/10.1016/j.jcrysgro.2003.09.022.

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42

Lin, Yi-Hsung, Subrata Das, Che-Yuan Yang, Jen-Cheng Sung, and Chung-Hsin Lu. "Phase-controlled synthesis of Cu2ZnSnS4 powders via the microwave-assisted solvothermal route." Journal of Alloys and Compounds 632 (May 2015): 354–60. http://dx.doi.org/10.1016/j.jallcom.2015.01.254.

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43

Tannert, Niels, Serkan Gökpinar, Emrah Hastürk, Sandra Nießing, and Christoph Janiak. "Microwave-assisted dry-gel conversion-a new sustainable route for the rapid synthesis of metal–organic frameworks with solvent re-use." Dalton Transactions 47, no. 29 (2018): 9850–60. http://dx.doi.org/10.1039/c8dt02029a.

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44

Yuvasravana, R., and P. P. George. "A Green Protocol for Synthesis of MAl2O4, [M=Cu and Co] Spinels Under Microwave Irradiation Method." International Journal of Nanoscience 16, no. 03 (2016): 1650033. http://dx.doi.org/10.1142/s0219581x16500332.

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Nanosized metal aluminates MAl2O4, [[Formula: see text] and Co] are synthesized from their nitrates solution by using pomegranate peel extract as fuel in microwave combustion. MAl2O4 [[Formula: see text] and Co] nanoparticles are grown in microwave assisted synthesis followed by annealing at 700[Formula: see text]C. The nanoparticles have been characterized by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), UV-VIS spectroscopy and photoluminescence (PL) spectroscopy. The PXRD analysis has confirmed their spinel composition. T

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45

Xiong, Weiwei, Ziyi Zhang, Yutao Huang, et al. "A microwave-assisted template-free route for large-scale synthesis of photoluminescent single crystal CsPbI3 nanotubes." CrystEngComm 22, no. 4 (2020): 623–27. http://dx.doi.org/10.1039/c9ce01722d.

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Taddei, Marco, Ferdinando Costantino, Riccardo Vivani, Stefano Sabatini, Sang-Ho Lim, and Seth M. Cohen. "The use of a rigid tritopic phosphonic ligand for the synthesis of a robust honeycomb-like layered zirconium phosphonate framework." Chem. Commun. 50, no. 43 (2014): 5737–40. http://dx.doi.org/10.1039/c4cc01253d.

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1,3,5-Tris(4-phosphonophenyl)benzene was synthesized via a microwave heating assisted route and was subsequently used for the preparation of a new zirconium phosphonate with honeycomb-like structure displaying remarkable thermal stability and hydrolysis resistance.

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Meier, Chris, Simon Weising, Patrick Dekiert, Dominique Schols, and Johan Neyts. "Synthesis of Enantiomerically Pure 1′,2′-cis-dideoxy, -dideoxydidehydro, -ribo and -deoxy Carbocyclic Nucleoside Analogues." Synthesis 50, no. 11 (2018): 2266–80. http://dx.doi.org/10.1055/s-0037-1609493.

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We describe a short and stereospecific synthesis of different series of 1′,2′-cis-disubstituted carbocyclic nucleoside analogues. All-natural nucleobases or their precursors are coupled in a microwave-assisted Mitsunobu-type reaction with enantiomerically pure (1R,2S)-2-(benzyloxymethyl)cyclopent-3-enol. By modifying the cyclopentene scaffold, our synthetic strategy gives access to a series of 1′,2′-cis-disubstituted carbocyclic nucleoside analogues of the dideoxy (dd), dideoxydidehydro (d4) or the ribo series. The ribo series is synthesized in a more convenient way compared to a previous rou

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Leyva-Noyola, F., and O. Solorza-Feria. "Microwave Assisted Synthesis of Ru3Pd6Pt Cathode Catalyst in a PEM Fuel Cell." Journal of New Materials for Electrochemical Systems 16, no. 3 (2013): 147–50. http://dx.doi.org/10.14447/jnmes.v16i3.3.

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Nanoparticles of Ru3Pd6Pt have been previously produced by different synthesis routes that involve high temperatures and relative high pressures and long time. The usage of a conventional microwave assisted synthesis reduces environmental risk impact as well as the cost effective production in large scale with minimum set up modifications. These features are the motivations for the use of microwaves in the synthesis of the Ru3Pd6Pt catalyst for PEM fuel cell applications to reduce the Pt loading. In this communication a tri-metallic electrocatalyst was produced by the reduction of the correspo

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Al-Mousawi, Saleh M., Morsy A. El-Apasery, and Najat H. Al-Kanderi. "Microwave-assisted organic synthesis: the Gabriel approach as a route to new pyrazolylhydrazonoazoles." Arkivoc 2008, no. 16 (2008): 268–78. http://dx.doi.org/10.3998/ark.5550190.0009.g25.

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Nissinen, Terhi A., Yohannes Kiros, Michael Gasik, and Markku Leskelä. "MnCo2O4Preparation by Microwave-Assisted Route Synthesis (MARS) and the Effect of Carbon Admixture." Chemistry of Materials 15, no. 26 (2003): 4974–79. http://dx.doi.org/10.1021/cm031093x.

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