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Relevant bibliographies by topics / Nitro compounds. Reduction (Chemistry)

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Academic literature on the topic 'Nitro compounds. Reduction (Chemistry)'

Author: Grafiati

Published: 4 June 2021

Last updated: 10 February 2022

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Journal articles on the topic "Nitro compounds. Reduction (Chemistry)"

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Sassykova, L. R., Y. A. Aubakirov, S. Sendilvelan, Zh Kh Tashmukhambetova, N. K. Zhakirova, M. F. Faizullaeva, A. A. Batyrbayeva, R. G. Ryskaliyeva, B. B. Tyussyupova, and T. S. Abildin. "Studying the Mechanisms of Nitro Compounds Reduction (A-Review)." Oriental Journal of Chemistry 35, no. 1 (January 21, 2019): 22–38. http://dx.doi.org/10.13005/ojc/350103.

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The article describes some variants of mechanisms of nitro compounds reduction, offered by authors in the scientific literature. The focus is on the description of the work of Kazakh and Russian chemists working in the field of catalysis. In most of the works, the classical scheme of the mechanism of the hydrogenation of Haber-Lukashevich nitrobenzene is confirmed and detailed by experimental methods. One of the interesting aspect of the article is description the mechanism of Ya.A. Dorfman which used the orbital theory of catalysis. The orbital approach of the Ya.A. Dorfman mechanism is constructed in the light of modern orbital representations and is valid for the hydrogenation of the nitro group on various catalysts. Among the discussed mechanisms are ideas of Haber, Debus, Jungers, V.P. Shmonina, Lukashevich, M. Geirovsky, Yu. B. Vasilyev, M.V. Klyuev, E.F. Weinstein, E. Gelder, Ya.A. Dorfman and others.

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Suzuki, Hitomi, Hajime Manabe, and Masahiko Inouye. "REDUCTION OF AROMATIC NITRO COMPOUNDS WITH SODIUM TELLURIDE." Chemistry Letters 14, no. 11 (November 5, 1985): 1671–74. http://dx.doi.org/10.1246/cl.1985.1671.

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Mahdavi, Farah, Thomas C. Bruton, and Yuzhuo Li. "Photoinduced reduction of nitro compounds on semiconductor particles." Journal of Organic Chemistry 58, no. 3 (January 1993): 744–46. http://dx.doi.org/10.1021/jo00055a033.

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Vygodskii, Ya S., L. I. Komarova, and Yu V. Antipov. "The reduction of aromatic nitro compounds by oxiranes." Russian Chemical Bulletin 43, no. 8 (August 1994): 1414–16. http://dx.doi.org/10.1007/bf00703708.

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Theodoridou, E., A. D. Jannakoudakis, P. D. Jannakoudakis, and S. Antoniadou. "Electrochemically oxidized carbon fibres as an adsorbent for the attachment of dissolved substances. Adsorption of nitro compounds and ion-exchange of heavy metals." Canadian Journal of Chemistry 69, no. 12 (December 1, 1991): 1881–85. http://dx.doi.org/10.1139/v91-272.

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The adsorption of several aromatic nitro compounds and the ion-exchange of heavy metal ions on electro-oxidized carbon fibres have been investigated using cyclic voltammetric and polarographic techniques. Electro-oxidation is performed by potentiostatic double pulse application. This procedure results in the generation of many functional —OH and —COOH groups with adsorptive and ion-exchanging properties.Multimolecular layers of adsorbed substances may be formed through a procedure of successive adsorption of the nitro-compound and electro-reduction to the corresponding amine, resulting in the attachment of considerable amounts of the nitro-compound to the carbon fibres.The ion-exchange capacity is estimated to be ca. 1 mequiv. g−1 and with slight deviations it follows the rank Ag, Cu, Cd, Pb, Hg. After the electro-reduction of the exchanged metal ions, the ion-exchange process can be repeated several times. This procedure is of importance for the removal of significant amounts of heavy and toxic metals from industrial waste waters. Key words: electro-oxidized carbon fibres, adsorption of aromatic nitro compounds, cation-exchange of heavy metals.

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Takeshita, Mitsuhiro, and Sachiko Yoshida. "Reduction of Hetero-aromatic Nitro Compounds with Baker's Yeast." HETEROCYCLES 31, no. 12 (1990): 2201. http://dx.doi.org/10.3987/com-90-5588.

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Sarmah, Parijat, and Dilip K. Dutta. "Manganese Mediated Aqueous reduction of Aromatic Nitro Compounds to Amines." Journal of Chemical Research 2003, no. 4 (April 2003): 236–37. http://dx.doi.org/10.3184/030823403103173624.

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Bock, Hans, and Ulrike Lechner-Knoblauch. "Radikalionen, 69 [1, 2] Die elektrochemische Reduktion aromatischer Nitro-Verbindungen in aprotischer Lösung / Radical Ions, 69 [1, 2] The Electrochemical Reduction of Aromatic Nitro Compounds in Aprotic Solution." Zeitschrift für Naturforschung B 40, no. 11 (November 1, 1985): 1463–75. http://dx.doi.org/10.1515/znb-1985-1108.

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The reduction potentials of 40 aromatic nitro compounds Rπ(NO2)n with Rπ = benzene, naphthalene, anthracene, fluorene and carbazole and n = 1 to 4 nitro groups are determined by cyclic voltammetry in DMF under aprotic conditions. The perturbation by the strongly electron accepting substituents can be rationalized via correlation with HMO eigenvalues. Based on reversibility criteria, the electrochemical behaviour is discussed and the compounds are classified with respect to reversible or irreversible one-electron transfer as well as up to 4 (quasi)-reversible reduction steps. The CV data measured can be used to predict redox reactions of aromatic nitro compounds in inert solvents.

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Pehlivan, Leyla, Estelle Métay, Stéphane Laval, Wissam Dayoub, Patrice Demonchaux, Gérard Mignani, and Marc Lemaire. "Iron-catalyzed selective reduction of nitro compounds to amines." Tetrahedron Letters 51, no. 15 (April 2010): 1939–41. http://dx.doi.org/10.1016/j.tetlet.2010.01.067.

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Formenti, Dario, Francesco Ferretti, Florian Korbinian Scharnagl, and Matthias Beller. "Reduction of Nitro Compounds Using 3d-Non-Noble Metal Catalysts." Chemical Reviews 119, no. 4 (December 5, 2018): 2611–80. http://dx.doi.org/10.1021/acs.chemrev.8b00547.

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Dissertations / Theses on the topic "Nitro compounds. Reduction (Chemistry)"

1

Cho, Jeongguk. "Porphyrin-catalyzed reduction of nitroaromatic compounds /." Access abstract and link to full text, 1992. http://0-wwwlib.umi.com.library.utulsa.edu/dissertations/fullcit/9307476.

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Park, Jonathan Taejoo. "Enzymatic reduction of nitro compounds to amines with nitroreductases." Diss., Georgia Institute of Technology, 2014. http://hdl.handle.net/1853/52267.

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NRs are enzymes that catalyze the reduction of nitroaromatics to their corresponding nitroso, hydroxylamine, and, in limited cases, amine They have gathered interest in many scientific communities, and are currently actively researched bioremediation and prodrug activation. Here we attempt to utilize them for the purpose of synthesizing substituted aromatic amines that are found in a number of active pharmaceutical ingredients (APIs). As NRs described in the literature have varying product distribution ranges (from those that produce hydroxylamine to others that yield amine) several similar and different NRs were studied for their selectivity. Additionally, a quantitative structure-activity relationship (QSAR) was determined to characterize the substrate specificity of NRs. To employ the use of flavoenzymes in synthesis, multiple reaction- and protein-engineering approaches were devised. One scheme was to establish an enzymo-chemical synthesis where NRs were paired with reducing agents for a chemical reduction. Another method was to create a monomeric NR through directed evolution from ER scaffolds for future immobilization applications. Protein engineering techniques were also utilized on NADH oxidases which we characterized and developed for nicotinamide cofactor regeneration. As a whole, this dissertation expands our current understanding on NRs and demonstrates the possibility of using several flavoenzymes in the synthesis of organic molecules.

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So, Sonia. "Boronate Urea Activation of Nitro Compounds." The Ohio State University, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=osu1395764122.

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Scherer, Michelle Marie. "Reduction of chlorinated aliphatic and nitro aromatic compounds at the Fe0-oxide-water interface /." Full text open access at:, 1998. http://content.ohsu.edu/u?/etd,201.

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Torano, Ronald. "Studies of new cyclisation reactions of heteroaromatic nitro and nitroso compounds." Thesis, University of Edinburgh, 1985. http://hdl.handle.net/1842/14557.

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Hyde, Andrew Richard. "Aspects of the chemistry of iron-nitrosyls." Thesis, University of St Andrews, 1985. http://hdl.handle.net/10023/14967.

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The work described in this thesis is a study of iron-sulphur-nitrosyls and related compounds. Chapter One is an introduction to the work presented. Chapter one is introduction to the work presented. Chapter Two is concerned with the analogous Fe2(SR)2(CO)6 and its conversion to Fe2(SR)2(NO)4. Chapter Three is concerned with an n.m.r. study of Fe2(SR)2(NO)4, Fe2X4(NO)4 and [Fe4X3(NO)7] (X=S, Se). Chapter four is concerned with an e.p.r. examination with an n.m.r. study of Fe2(SR)2(NO)4, Fe2X4(NO)4 [Fe4X3(NO)7] (X=S,Se). Chapter four is concerned with an e.p.r. examination of Fe2(SR)2(NO)4 and bridging ligand exchange reactions. Chapter Five is concerned with a similar examination of Fe2I2(NO)4.Chapter six is concerned with an examination of ligand exchange processes in Fe4S4(NO)4 and [Fe4S4(NO)4]. Chapter Seven is concerned with an investigation of iron-sulphur protein models and their conversion to iron-nitrosyls.

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Baralt, Eduardo. "Hydrogenation of Nitro Compounds to Amines Using Polymer Bound Catalysts." TopSCHOLAR®, 1985. http://digitalcommons.wku.edu/theses/1883.

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A polymer bound catalyst is a relatively new type of catalyst. The basis of polymer bound catalysis lies in the chemical attachment of a homogeneous catalyst to a solid support, in our case, polystyrene. Applications of polymer bound catalysts started in the late 1960’s, and have been used in several types of reactions. In some cases such a catalyst offers a series of advantages over the classical models of catalysis, homogeneous and heterogeneous. The hydrogenation of various aromatic and aliphatic nitro compounds, such as nitro-benzene and 2-nitropropane, were performed successfully. The hydrogenation activity in most cases was high, and in some reactions the catalyst was able to hydrogenate molecules that the analogous homogeneous catalyst could not. Different metals; specifically palladium, platinum, nickel, and rhodium, were attached to the polymer and the effects of varying the metal on the activity were studied. Palladium supported catalysts with anthranilic acid as a polymer supported ligand were found to be more active and selective than palladium catalysts with a bipyridyl ligand. Substitution on the aromatic ring of the substrate alters the reaction rate. Steric effects have a large influence over the catalytic activity. Electron withdrawing groups do not alter reaction rates greatly, while resonance effects can increase the rate of reaction. Finally the effect of the reaction conditions (temperature, pressure and time) on the catalyst activity were analyzed.

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Duffield, Gaynor Louise. "Some studies of the reactions of carbon nucleophiles with aromatic nitro compounds." Thesis, Durham University, 1996. http://etheses.dur.ac.uk/5191/.

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Some reactions of aromatic nitro-compounds with carbon nucleophiles have been investigated. The techniques used include NMR spectroscopy, UV-visible spectroscopy and stopped-flow spectrophotometry. The initial rapid reactions of carbanions derived from ring-substituted phenylacetonitriles with 1,3,5-trinitrobenzene yield σ-adducts. Carbanions were generated from the phenylacetonitriles by reaction with sodium methoxide in methanol. Values of the equilibrium constants for the deprotonation reaction were determined spectrophotometrically. Rate constants for the σ-adduct forming reactions were measured in methanol using the stopped-flow method. With increasing carbanion reactivity rate constants for the C-C bond forming reaction increase to a limit of circa 10(^9) dm(^3) mol(^-1) s(^-1) close to the diffusion limit. Data were also obtained for reaction of the carbanions with 4-nitrobenzofuroxan and with 4-nitrobenzofurazan.An interesting slower reaction was observed in the reaction of carbanions with 1,3,5- TNB, 4-nitrobenzofuroxan and 4-nitrobenzofurazan. This yields coloured products and the nature of the process has been investigated. Attempts have been made to isolate the σ-adducts formed from carbanions. The adduct formed from 1,3,5-trinitrobenzene and phenylacetonitrile in the presence of triethylamine has been produced in crystalline form. NMR measurements in situ have indicated the formation of adducts from 4-nitrobenzofuroxan and from 4-nitrobenzofiirazan with deuterated nitromethane in the presence of triethylamine.

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Li, Zhao. "The Kinetics and Mechanisms of Some Fundamental Organic Reactions of Nitro Compounds." DigitalCommons@USU, 2012. https://digitalcommons.usu.edu/etd/1407.

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The central topic of this dissertation is to seek the answer to the question: Is the single transition state model appropriate for (1) the proton transfer reactions of nitroalkanes and (2) the aromatic nucleophilic reactions of trinitroarenes? If not, what are the real mechanisms? This objective has been accomplished by careful kinetic and mechanistic studies which take advantage of modern digital acquisition of absorbance - time data, combined with extensive new data analysis of results from pseudo-first-order kinetic measurements. Several new analysis procedures for pseudo-first-order kinetics that are capable of distinguishing between single-step and multi-step mechanisms have been introduced and intensively confirmed during the application in the kinetic study of the target reactions. The procedures include (1) half-life dependence of apparent rate constant, (2) sequential linear pseudo-first-order correlation, (3) approximate instantaneous rate constant analysis, and (4) time-dependent apparent kinetic isotope effects. Various conventional and nonconventional pseudo-first-order kinetic analyses of the reactions of nitroalkanes in aqueous solutions revealed that the reactions are complex and involve kinetically significant intermediates. The spectral evidence for the formation of reactive intermediates was obtained by carrying out the kinetic experiments at the isosbestic points where changes in reactant and product absorbance cancel. The apparent deuterium kinetic isotope effects studies indicated that the deuterium kinetic isotope effects are not associated with the formation of the intermediates. The observations of anomalous Brønsted exponents previously found for this reaction series could be rationalized well with the complex mechanisms proposed in this work, which indicate that the nitroalkane anomaly does not exist, but arises from an interpretation based upon the incorrect assumption that the reactions follow a simple one-step mechanism. Simulations revealed that the generally accepted competitive mechanism was not appropriate to describe the Meisenheimer complex formation during the reaction of 2,4,6-trinitroanisole with methoxide ion in methanol. This conclusion is supported by the conventional pseudo-first-order kinetic analysis. A reversible consecutive mechanism that accounts for the kinetic behavior has been proposed, which involves an intermediate dianion complex that is formed reversibly from the initial 1,3-σ-complex, and then eliminates methoxide ion to form the 1,1-σ-complex product.

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Eltayeb, M. A.-Z. "Aspects of the detection and determination of aromatic nitro-compounds for forensic purposes." Thesis, Queen's University Belfast, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.374190.

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Books on the topic "Nitro compounds. Reduction (Chemistry)"

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Cenini, Sergio. Catalytic reductive carbonylation of organic nitro compounds. Dordrecht: Kluwer Academic Publishers, 1997.

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Hudlicky, Milos. Reductions in organic chemistry. 2nd ed. Washington, DC: American Chemical Society, 1996.

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Oxidation and reduction in organic synthesis. New York: Oxford University Press, 2000.

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Hudlický, Miloš. Reductions in organic chemistry. 2nd ed. Washington, D.C: American Chemical Society, 1996.

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Valentin, Lopyrev, ed. Nitroazoles: Synthesis, structure and applications. Dordrecht: Springer, $c c2009., 2009.

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Larson, G. L. Ionic and organometallic-catalyzed organosilane reductions. Hoboken, N.J: Wiley, 2010.

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Mennekes, Theodor. Zur Reduktion von Dihalogenorganylboranen mit Alkalimetallen. Aachen: Verlag Shaker, 1992.

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Penne, J. Seyden. Reductions by the alumino- and borohydrides in organic synthesis. Weinheim: VCH Verlagsgesellschaft, 1991.

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Lappin, Graham. Redox mechanisms in inorganic chemistry. New York: Ellis Horwood, 1994.

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Reductions by the alumino- and borohydrides in organic synthesis. 2nd ed. New York: Wiley-VCH, 1997.

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Book chapters on the topic "Nitro compounds. Reduction (Chemistry)"

1

Lockhart, I. M. "Nitro- and Aminochromans." In Chemistry of Heterocyclic Compounds: A Series Of Monographs, 189–250. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2008. http://dx.doi.org/10.1002/9780470187098.ch6.

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Vogt, R. A., S. Rahman, and C. E. Crespo-Hernández. "Structure–Activity Relationships in Nitro-Aromatic Compounds." In Practical Aspects of Computational Chemistry, 217–40. Dordrecht: Springer Netherlands, 2009. http://dx.doi.org/10.1007/978-90-481-2687-3_10.

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Redington, Patrick K., and Jan W. Andzelm. "Density Functional Calculations on Nitro Compounds (Geometries)." In Density Functional Methods in Chemistry, 411–18. New York, NY: Springer New York, 1991. http://dx.doi.org/10.1007/978-1-4612-3136-3_27.

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Iinuma, Yoshiteru, and Hartmut Herrmann. "Nitro- and Nitro-Oxy-Compounds in Multiphase Particle Chemistry: Field and Analytical Studies." In Disposal of Dangerous Chemicals in Urban Areas and Mega Cities, 185–93. Dordrecht: Springer Netherlands, 2012. http://dx.doi.org/10.1007/978-94-007-5034-0_15.

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Belen'Kii, L. I., and Y. A. L. Gol'Dfarb. "Reduction and Desulfurization of Thiophene Compounds." In Chemistry of Heterocyclic Compounds: A Series Of Monographs, 457–570. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2008. http://dx.doi.org/10.1002/9780470187234.ch6.

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Lund, Henning. "Electrochemical Reduction of Some Sulfur Compounds." In Sulfur-Centered Reactive Intermediates in Chemistry and Biology, 93–102. Boston, MA: Springer US, 1990. http://dx.doi.org/10.1007/978-1-4684-5874-9_10.

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Rabideau, Peter W. "Dissolving-Metal Reduction of Polynuclear Aromatic Compounds in Liquid Ammonia." In Advances in Chemistry, 73–87. Washington, DC: American Chemical Society, 1987. http://dx.doi.org/10.1021/ba-1988-0217.ch005.

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Mizzoni, Renat H. "Nitropyridines and Reduction Products (Except Amines)." In Chemistry of Heterocyclic Compounds: A Series Of Monographs, 1–40. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2008. http://dx.doi.org/10.1002/9780470186725.ch1.

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Mizroni, Renat H. "Nitropvridines and their Reduction Products (Except Amines)." In Chemistry of Heterocyclic Compounds: A Series Of Monographs, 469–545. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2008. http://dx.doi.org/10.1002/9780470186657.ch6.

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Nakagome, Takenari. "Nitropyridazines and Their Reduction Products (Except Amines)." In Chemistry of Heterocyclic Compounds: A Series Of Monographs, 629–73. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2008. http://dx.doi.org/10.1002/9780470186985.ch7.

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Conference papers on the topic "Nitro compounds. Reduction (Chemistry)"

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Naimi-Jamal, Mohammad Reza, arefeh dadras, Firouz Matloubi Moghaddam, and Seyed Ebrahim Ayati. "Nitro compound reduction in the presence of robust palladium immobilized on modified magnetic Fe₃O₄ nanoparticles as a recoverable catalyst." In The 21st International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 2017. http://dx.doi.org/10.3390/ecsoc-21-04825.

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Pelipko, Vasilii, and Sergey Makarenko. "ALKYL-3-NITRO- AND 3-BROMO-3-NITROACRYLATES - ORIGINAL UNSATURATED NITRO-COMPOUNDS." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m750.aks-2019/190-196.

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Anisimova, Nadezhda, and Alena Kuzhaevac. "1-NITRO- AND 1-BROM-1-NITRO-3,3,3-TRICHLOROPROPENES IN REACTION WITH DIAZOMETAN." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m753.aks-2019/209-211.

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Sysolyatin, S., A. Kalashnikov, V. Malykhin, A. Paromov, and I. Shchurova. "CHEMISTRY AND TECHNOLOGY OF HIGH-ENERGY COMPOUNDS." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m717.aks-2019/34.

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Drokin, R., D. Gazizov, D. Tiufiakov, E. Voinkov, E. Gorbunov, E. Ulomsky, G. Rusinov, and V. Rusinova. "POTASSIUM SALTS OF NITROCARBONYL COMPOUNDS IN THE SYNTHESIS OF NITROGEN-CONTAINING HETEROCYCLIC COMPOUNDS." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m749.aks-2019/187-189.

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Ustinov, Ilya, Nikolaj Khlytin, Yurij Atroshchenko, and Irina Shahkeldyan. "NEW THIAZOL DERIVATIVES CONTAINING NITRO QUINOLINE FRAGMENT." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m797.aks-2019/383-384.

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Ovcharenko, Victor. "MULTISPIN COMPOUNDS CONTAINING NITROGEN-OXYGEN FRAGMENTS." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m715.aks-2019/24-26.

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Rusinov, V., V. Charushin, and О. Chupakhina. "NITRO SYNTHONS IN THE SYNTHESIS OF NITRO DERIVATIVES OF AZOLO[1,5-а]PYRIMIDINES AND AZOLO[5,1-с]-1,2,4-TRIAZINES." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m720.aks-2019/47-52.

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Grigoreva, Anastasiya, Aleksandr Kotov, and Аnton Shetnev. "THORPE REACTION STUDY INVOLVING NITRO-SUBSTITUTED AROMATIC NITRILES." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m762.aks-2019/237-240.

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Glukhacheva, Vera, and Sergey Ilꞌyasov. "SYNTHESIS AND PROPERTIES OF NITRO DERIVATIES OF HETEROCYCLIC ANTRACENES." In Chemistry of nitro compounds and related nitrogen-oxygen systems. LLC MAKS Press, 2019. http://dx.doi.org/10.29003/m729.aks-2019/97-99.

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Reports on the topic "Nitro compounds. Reduction (Chemistry)"

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Shukla, Manoj K., Luidmyla K. Sviatenko, Sergly I. Okovytyy, Danuta Leszczynska, and Jerzy Leszczynski. Catalytic Role of Solvated Electron in the Spontaneous Degradation of Insensitive Munition Compounds : Computational Chemistry Investigation. Engineer Research and Development Center (U.S.), July 2021. http://dx.doi.org/10.21079/11681/41122.

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The DNAN (2,4-dinitroanisole), NTO (3-nitro-1,2,4-triazol-5-one), and NQ (nitroguanidine) are important insensitive energetic materials used in military applications. They may find their way to the environment during manufacturing, transportation, storage, training, and disposal. A detailed investigation of possible mechanisms for self-degradation of radical-anions formed by addition of solvated electron to DNAN, NTO, and NQ species was performed by computational study using the PCM(Pauling)/M06-2X/6-311++G(d,p) approach. Obtained results suggest that only NQ radical-anion is able for self-degradation by elimination of nitrite anion. Formation of urea radical on the earlier stage of the NQ radical-anion degradation was also predicted.

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